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《Science of Sericulture》 2007-01
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Preparation of Silk Fibroin-Chitosan Blend Membrane and its Property Mensuration

CHEN Chun-Hua1 ZHU Liang-Jun2 ZOU Feng-Zhu1*(1College of Forestry,Shandong Agricultural University,Taian Shangdong 271018,China;2College of Science of Animal,Zhejiang University,Hangzhou 310029,China)  
In order to improve the property of silk fibroin membrane,by utilizing of orthogonal design of L32(8×48)the blending experiments of silk fibroin with chitosan were carried out.And the effects of different conditions including concentration,temperature and pH etc. on the property of blend membrane were studied.The results showed that swelling rate ranged between 43.00% and 248.94%,water solubility ranged between 43.06% and 64.56%,while breathe freely rate ranged from 36.81% and 55.39%,and modulus,relative break strength and relative break strain were from 6.35 to 68.80 N/mm,30.85 to 67.83 N/mm and 28.05 to 230.47,respectively.Analysis by infrared spectrum indicated that silk fibroin and chitosan were physically blended and compatible with each other.The preliminary optimized combine conditions of composite were confirmed as follows: silk fibroin content is 70% or 55%,temperature is 40℃,concentrations both of glutaraldehyde and glycerol are 0.3%.
【CateGory Index】: TS149
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