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《Technical Textiles》 2013-08
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LC-MS/MS determination of aloe constituents in textiles

Zhou Yu,Liao Guoying,Yang Xinhui,Zhang Yulian(Guangzhou Fiber Product Testing Institute)  
An ultra effective liquid chromatography-tandem mass spectrometry(LC-MS/MS) method has been developed for determinating the contents of aloin,aloe-emodin and chrysophanol in textiles.The samples were prepared by ultrasonically extracting using methanol at 60 ℃ for 30 min.The LC separation was performed on an Agilent XDB-C18 column(2.1 mm×150 mm,3.5 m) using 10 mmol/L ammonium acetate as solution(pH=5.75) and acetonitrile as the mobile phase in a gradient elution mode.The analyses were tested by a triple-quadrupole mass spectrometer in the multiple reaction monitoring(MRM) mode using electrospray source with negative mode,and quantified by external standard method.The average recoveries of analyses in textile samples at the three spiked levels were in the range of 85.5%~99.9% with the relative standard deviations being 1.76%~5.92%.The method was proved to be rapid,sensitive,accurate and reproducible and can be applied to the trace analysis of aloe constituents in textiles.
【Fund】: 国家质监总局科技计划项目(2010QK093)
【CateGory Index】: TS107;O657.63
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