Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Technical Textiles》 2013-08
Add to Favorite Get Latest Update

LC-MS/MS determination of aloe constituents in textiles

Zhou Yu,Liao Guoying,Yang Xinhui,Zhang Yulian(Guangzhou Fiber Product Testing Institute)  
An ultra effective liquid chromatography-tandem mass spectrometry(LC-MS/MS) method has been developed for determinating the contents of aloin,aloe-emodin and chrysophanol in textiles.The samples were prepared by ultrasonically extracting using methanol at 60 ℃ for 30 min.The LC separation was performed on an Agilent XDB-C18 column(2.1 mm×150 mm,3.5 m) using 10 mmol/L ammonium acetate as solution(pH=5.75) and acetonitrile as the mobile phase in a gradient elution mode.The analyses were tested by a triple-quadrupole mass spectrometer in the multiple reaction monitoring(MRM) mode using electrospray source with negative mode,and quantified by external standard method.The average recoveries of analyses in textile samples at the three spiked levels were in the range of 85.5%~99.9% with the relative standard deviations being 1.76%~5.92%.The method was proved to be rapid,sensitive,accurate and reproducible and can be applied to the trace analysis of aloe constituents in textiles.
【Fund】: 国家质监总局科技计划项目(2010QK093)
【CateGory Index】: TS107;O657.63
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 6 Hits
1 Yu Jia and Wu Weiwei (Zhejiang University of Sciences)Jin Jianping and Ye Yanyan (Huzhou Xiangshun Ecological Fabrics Development Co., Ltd. );Antibacterial function of aloe and its application in the fabrics[J];Technical Textiles;2008-02
2 DENG Jun wen( The University Journal Editing Division, Foshan University, Foshan 528000 ,China);The chemical compositions of Aloe and its pharmacological action[J];JOURNAL OF FOSHAN UNIVERSITY(NATURAL SCIENCE EDITION);2000-02
3 Li Yunzheng, Qin Haiyuan, Wang Qinghua (The Research Center of Material Science, Beijing Institute of Technology, Beijing, l00081 );Progress in Research and Development of Aloe Vera[J];CHEMICAL INDUSTRY AND ENGINEERING PROGRESS;2000-02
4 DUAN Hui-guo~1, QING Dong-hong~1, HU Rong~(1.2) (1. Department of Chemistry and Life Science,Neijiang Teachers College,Neijiang, Sichuan 641112, China; 2.Editorial Department of Journal,Neijiang Teachers College,Neijiang, Sichuan 641112, China);The Chemical Compositions and Their Effects in Aloes[J];Journal of Neijiang Teachers College;2004-06
5 Ai-hua LI,Ai-guo ZHAO,Chang-zhi SU,(Technical Centre,Yuyue Househole Textiles Company Limited,Binzhou,Shandong);Functional Finishing of Househole Textiles with Aloe[J];Textile Dyeing and Finishing Journal;2010-05
6 Li Xiaodi (Shantou Grand Louis Paris Cosmetic Co., LTD.515144);Aloe and Cosmetic[J];Flavour Fragrance Cosmetics;2001-01
Chinese Journal Full-text Database 10 Hits
1 Pan Hong(Shaoxing Branch of Zhejiang Econamia&Trade Polytechnic);The Health Protectional Virtue and Exploiture of Aloe[J];Anhui Agricultural Science Bulletin;2007-23
2 HUANG You-qin et al(Department of Food Engineering,Guangxi Agricultural Professional Technology College,Nanning,Guangxi 530007);Development of the Suspended Beverage of the Aloe Mesophyll[J];Journal of Anhui Agricultural Sciences;2010-20
3 WANG Jun-jie et al(College of Material Sciences and Chemical Engineering,Hainan University,Danzhou,Hainan 571737);Research Progress on Extraction and Detection and Medicinal Value of Anthrone Compounds in Aloe[J];Journal of Anhui Agricultural Sciences;2010-21
4 ZHU Jun-ling et al(College of Food Science and Engineering,Shanxi Agricultural University,Jingzhong,Shanxi 030801);Optimization of Supercritical CO_2 Fluid Extraction Process for Aloe Polysaccharide[J];Journal of Anhui Agricultural Sciences;2011-10
5 DAI Hong, ZHANG Zong-cai, ZHANG Xin-shen, LI Bo (Key Laboratory of Leather Chemistry and Engineering of Ministry of Education, Sichuan University, Chengdu 610065 ,China);Isolation and Extraction of Polysaccharide in Aloe[J];Amino Acids & Biotic Resources;2004-01
6 WANG Shuanghua, ZHANG Heng, DUAN Chengjin, ZHANG Jun(Material Science and Engineer School, Zhengzhou University, Zhengzhou 450052);Preparation Technology and Applications of Microcapsule[J];Materials Review;2006-S2
7 WU Jia-mei~1, LIU Zhao-pu~(1*), LIU Ling~1, DENG Li-qun~2(1 College of Resource and Environment, Nanjing Agricultural University, Nanjing 210095,China;2 Science and Technology Bureau of Jianye District, Nanjing 210087,China);Response of Aloe vera Seedlings to Seawater[J];Acta Botanica Boreali-occidentalia Sinica;2005-08
8 WANG Chang-kang1,JIA Hong-qiang1,TONG Jian-ming2,GAO Wei-wei3,SA Ren-na2,ZHANG Qi2 (1.College of Animal Science,Fujian Agriculture and Forestry University,Fuzhou, Fujian 350002,China;2.Institute of Animal Science,Chinese Academy of Agricultural Sciences,Beijing 100094,China;3.Institute of Medicinal Plant Development,Peking Union Medical College,Beijing 100094,China);Effect of aloe powder and extract on production performance and immune function of broiler chickens[J];Journal of Fujian Agriculture and Forestry University(Natural Science Edition);2007-06
9 LIU Hao1,TONG Jian-ming2,JIA Hong-qiang1,DONG Xiao-fang2,WANG Chang-kang1,GAO Wei-wei3,SA Ren-na2,ZHANG Qi2(1.Fujian Agriculture and Forestry University,Fuzhou,Fujian 350000,China; 2.State Key Laboratory of Animal Nutrition,Institute of Animal Science,CAAS,Beijing 100094,China;3.Institute of Medicinal Plant Development,Chinese Academy of Science,Beijing 100094,China);Effect of aloe powder on immunity and productivity of male and female broilers[J];Fujian Journal of Agricultural Sciences;2007-03
10 LIN Xin\|hua, CHEN Jun, CHEN Wei, HUANG Li\|ying, LUO Hong\|bin Division of Pharmacy, Fujian Medical University, Fuzhou 350004, China;Extraction and Determination of Polysaccharide from Aloe[J];Journal of Fujian Medical University;2003-02
China Proceedings of conference Full-text Database 2 Hits
1 Zheng Wei Ren Yuanlin School of Material Science and Chemical Engineering,Tianjin Polytechnic University;Trends of new skin care fibre and its fabric[A];[C];2007
2 HE Xian-jun, ZHANG Xue-dan, LU Guang-pu, YIN Fang (Center of Biotechnology Experiment, Beijing City University, Beijing 100094, China);Advances of Bacteriostasis of Aloe[A];[C];2008
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 HOU Dong yan HUI Rui hua LI Tie chun (Department of Chemistry,Anshan Normal University,Anshan Liaoning 114005,China);Research Progress of Aloes[J];Journal of Anshan Teachers College;2002-03
2 Jia Jicheng;Gao Yixiang College of Chemical Engineering College of Textile Engineering;Research on the Polysaccharide of Chinese Aloe gel[J];Journal of Beijing Union University;1993-01
3 DENG Jun wen( The University Journal Editing Division, Foshan University, Foshan 528000 ,China);The chemical compositions of Aloe and its pharmacological action[J];JOURNAL OF FOSHAN UNIVERSITY(NATURAL SCIENCE EDITION);2000-02
4 Wang Hua;Health Care & Anti-bacteria Finish of Traditional Natural Plant Medicine and Textile[J];Journal of Textile Research;2004-01
5 Li Jinxin Feng Mei (Ninxia Agricultural College, Yonging Ningxia, 750105);MEDICINAL EFFECT AND DEVELOPMENT OF BARBADOS ALOE[J];JOURNAL OF NINGXIA AGRICULTURAL COLLEGE;1999-04
6 CHANG Ying, LI Long(Xi'an University of Engineering Science & Technology,Xi'an 710048,China);Application of aloe in functional wool knitting wears[J];Wool Textile Journal;2005-07
7 Yan Dongmei;Study on the antibacterial action of Aloe[J];SCIENCE AND TECHNOLOGY OF FOOD INDUSTRY;1998-03
8 Zhang Xiaohua Ye Yibing Li Han (Beijing Institute of Light Industry Beijing 100037);The Application of High Pressure Liquid Chromatography in Diagnosing the Special Property of Aloe──"E-Peak[J];FLAVOUR FRAGRANCE COSMETICS;1999-01
9 Hao Liqing (Yunnan Province S & T Information Research Institute Kunming 650051) Hao Wei (Yunnan University Kunming 650091);Industrial Developmental Prospects of Aloe[J];FLAVOUR FRAGRANCE COSMETICS;1999-02
10 Lin Xiang Yun (Xiamen Peony Perfume & Chemicals Industry Co.Ltd, 361006);Membrane Separation Technology Used in Aloe Gel Processing[J];FLAVOUR FRAGRANCE COSMETICS;1999-04
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved