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Synthesis of water-based macromolecular auxiliary agent of maleic anhydride-ethanolamine-styrene for pigments dispersion

DIAO Li,CAO Ya-feng College of Light Industry and Chemical Engineering,Dalian Polytechnic University,Dalian 116034,China  
A polycarboxylate type maleic anhydride- ethanolamine-styrene(MA-EA-St) macromolecular dispersant was synthesized by solution polymerization with ethyl acetate as solvent,maleic anhydride,ethanol amine,and styrene as monomers,and benzoyl peroxide as initiator.The influence of polymerization temperature and time,initiator dosage,and the molar ratio of acylated maleic anhydride to styrene on the suspensibility of TiO2 particles was studied.The relatively good polymerization reaction conditions were obtained as follows: molar ratio of acylated maleic anhydride to styrene 1.25,polymerization temperature 75 °C,polymerization time 5 h,and initiator dosage 2wt%(relative to the total weight of monomers).The suspensibility of TiO2 particles is 97.42%,which is up to good dispersion effect when the dosage of MA-EA-St dispersant obtained under the above conditions is 2.5 g/L.
【CateGory Index】: TQ630.49
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