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《中国纺织大学学报》 2000-05
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Determination of Trace Vanadium (V) Using Ethylvoilet and Potassium Bromate Catalytic Kinetic Spectrophotometry

Cheng Wei (College of Xuzhou Chemical Industrial, Xuzhou. 221006 )  
A catalytic procedure for determination of trace vanadium is proposed based on vanadium catalyzed potassium bromate ethylvoilet redox reaction in HCI medium. The calibration graph is linear for a range q 0.2 ~ 1.6 μg/L, and the detection limit is 0.2 fig/L, RSD is 1.24% ~ 2.78% . There is not obvious interference with 50 times of Mn~(2+)?Cu~(2+)? Fe~(2+)?Fe~(3+)?Cr~(3+)?Pb~(2+) and 100 times of K~+? Na~+?Ca~(2+)?Mg~(2+)?Cl~-?I~- .The procedure has been used to determine water sample directly.
【CateGory Index】: O657.3
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