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《Journal of Dalian Medical University》 2003-01
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Study of advantage on microwave irradiation technology of synthesizing oxaprozine

DENG Sa , TIAN Yan (Department of Pharmaceutical Chemistry, Dalian Medical University, Dalian 116027,China)  
To compare the advantage and shortage of microwave irradiation with common method on synthesizing oxaprozine. Oxaprozine was synthesized by the microwave irradiation in microwave reaction instrument and by the common method in the flask. The yield of the oxaprozine was 83% in17 min by the microwave irradiation while the yield was 65% in 5 h by the common method.[Conclusions] The microwave irradiation expend fewer time and energy and get higher yield than the common method.
【CateGory Index】: R914
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2 CHEN Bang-Yin~* ZHANG Han-Ping DING Wei-Pei (Dept.of Pharmacy,Tongji Medical University,Wuhan 430030);SYNTHESIS OF OXAPROZINE[J];Chinese Journal of Pharmaceuticals;1991-05
Chinese Journal Full-text Database 10 Hits
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2 NIE JinyuanaZHNAG Mengjuna~bWU Shironga LI Zhiliang~(*a)(aCollege of Chemistry and Chemical Engineering (CCCE), Chongqing University CQU, Shichuang Chongqing 400044; b Faculty of Clinical Analytical Sciences, The third Military Medical University, Shichuang 400038; *Correspondence author);Methods and techniques of microwave radiation as applied in research and development of traditional Chinese medicines[J];Journal of Changsha University;2003-04
3 PENG Long1, XU Guang-liang1, LIU Li2 1. College of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang 621010, China; 2. Southwest Institute of Applied Magnetics, Mianyang 621000,China;Advances in Preparation of Magnetic Powders by Hydrothermal Method[J];Journal of Magnetic Materials and Devices;2005-03
4 DENG Hong, JIANG Bin, ZENG Juan, LI Yang, LI Yan-rong, WANG En-xin (Institute of Information Materials Engineering, UEST of China, Chengdu Sichuan 610054);Microwave hydrothermal synthesis PZT ceramic powder[J];Electronic Components $ Materials;2001-02
5 Cui Hui; Liang Yizeng (Institute of Chemometrics and Chemical Sensing Technology , Hunan University, Changsha 410082 );Modern Analytical Chemistry and Chemometrics[J];Chinese Journal of Analytieal Chemistry;1996-08
6 Wang Yong, Zhang Zhuoyong, Liu Sidong, Guo Liping (Department of Chemistry, Northeast Normal University, Changchun 130024);Non-linear Calibration in Analytical Chemistry[J];Chinese Journal of Analytieal Chemistry;1998-09
7 Lü Jian-Feng, Dai Lian-Kui (National Key Lab of Industrial Control Technology, Zhejiang University, Hangzhou 310027);Improved Weighted Least Squares Support Vector Machines Algorithm and Its Applications in Spectroscopic Quantitative Analysis[J];Chinese Journal of Analytical Chemistry;2007-03
8 Liang Liang Cui Yingde Luo Zongming Dept.of Chemical Engineering.GDUT,Guangzhou 510090;Study on Preparation of Chitosan with Microwave New Technology[J];JOURNAL OF GUANGDONG UNIVERSITY OF TECHNOLOGY;1999-01
9 Zhang Zhibin Zhan Ding Lu Ping (Institute of Engineering, Yangzhou University, Yangzhou ,225009);The Microwave of Billion Hz and low power Catalyzing the Synthesis of Benzonic Esters[J];Guangdong Chemical Industry;2000-03
10 Long Jinqiao,Feng Lu,He Yanying,Wei Xiuli(Deptarment of Chemistry,Guangxi Youjiang Teachers College for Nationlities,Baise,Guangxi,533000,China);Synthesis of Isobutyl p-Hydroxybenzoate with Catalysis and Microwave in Sealed Jar[J];Guangxi Sciences;2005-04
China Proceedings of conference Full-text Database 1 Hits
1 Jiang Fengchao Wang Jing School of pharmacy, Tongji Medical college of HUST, Wuhan, China (430030);The structure modification of Oxaprozine[A];[C];2006
【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 CHEN Bang-Yin~* ZHANG Han-Ping DING Wei-Pei (Dept.of Pharmacy,Tongji Medical University,Wuhan 430030);SYNTHESIS OF OXAPROZINE[J];Chinese Journal of Pharmaceuticals;1991-05
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