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《GEOCHIMICA》 1996-06
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SIMULTANEOUS AND PRECISE DETERMINATION OF 40 TRACE ELEMENTS IN ROCK SAMPLES USING ICP-MS

Liu Ying; Liu Haichen; Li Xianhua (Guangzhou institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640)  
A simple method for the simultaneous and precise analysis of 40 or more trace elements in geological rock samples using ICP-MS has been developed in our laboratory with newly installed PE Elan 6000 ICP-MS. Rock samples were dissolved using distilled HF+HNO3 in screw-top Teflon beakers for 7-10 days at 100℃. Such a sample digestion process can minimize the contamination and lower the analytical blank and limits of detemination. The calibration solution was prepared from a USGS natural reference material BCR-l which can match the matrix of the unknown samples. Our new developed method for analysis of trace elements is characterized by its simple, straightforward sample preparation, data reduction and improved precision. The relative differences in concentration of the most trace elements between this work and“compiled”values for the standard rock samples are less than 5%.
【Fund】: 中国科学院广州地球化学研究所所长基金
【CateGory Index】: P584
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