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《地球科学》 2000-02
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ICP-MS ANALYTICAL RESEARCH INTO 40 TRACE AND ULTRA-TRACE ELEMENTS IN GEOLOGICAL SAMPLES

Hu Shenghong 1 Chen Aifang 2 Lin Shoulin 2 Yuan Honglin 1 Gao Shan 1 (1. Faculty of Earth Sciences, China University of Geosciences, Wuhan430074, China; 2. Faculty of Material Sciences and Chemical Engineering, China University of Geosciences, W  
The analytical method of major, trace and ultra_trace elements is applied to geological samples using ICP_MS. In order to minimize matrix effects of inter_elements, the matrix_matched calibration solutions were prepared, simulating the composition of natural rocks obtained from statistically_calculated average values of 20 geological samples. The resulting values are then normalized. Two separate internal standards of 115 In_ 103 Rh are selected to compensate the drift of analytical signals. Polyatomic ion interference is calibrated by measuring the oxides (MO +) and hydroxides (MOH +) with individual element solution for the ratio of MO +/M + and MOH +/M + and the concentrations are then equivalently calculated. The proposed method is applied to the analysis of seven standard reference materials. For the most trace elements, the relative errors between this work and the recommend values are greater than 10% and the relative standard deviations are greater than 5%.
【Fund】: 国家自然科学基金项目!(No .49973 0 2 6);; 教育部跨世 纪人才培养计划基金项目
【CateGory Index】: P584
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