Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of The Fourth Military Medical University》 2004-07
Add to Favorite Get Latest Update

Quality standard of Huatengzi Granules

WANG Xiao Juan 1, ZHU Ling Zhen 2, LIU Jie Zhong 1, WANG Rong 1 1Departmeny of Pharmacy, College of Stomatology, 2Institution of Materia Medca, Fourth Military Medical University, Xi’an 710033, China  
AIM: To determine the content of emodin and oleanolic acid in Huatengzi Granules (HTZG) by HPLC. METHODS: ODS C 18 column was used to determine emodin, the methanol and phosphoric acid aqueous solution ratio of the mobile phase being 90∶10 and the methanol water ratio of the mobile phase being 90∶10 in determining oleanolic acid. The detection wave length was 290 nm and 215 nm, respectively. RESULTS: A good linear relationship was obtained between the peak area and the concentration of emodin from 0.1314 to 0.8760 μg ( r =0.9997). The average recovery rate of emodin was 99.56% and RSD was 2.20% . A good linear relationship was obtained between the peak area and the concentration of oleanolic acid from 1.17 to 7.80 μg ( r =0.9998). The average recovery rate of emodin was 100.38% and RSD was l.45%. CONCLUSION: The method employed in this study can be used in quality control of HTZG.
【CateGory Index】: R286.0
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 1 Hits
1 HUANG Wen LI Ming LIN Zhong-ze LI Zhuo-ming LAI Xiao-ping SU Zi-ren~*(Guangzhou University of Traditional Chinese Medicine,Guangzhou 510405,China);HPLC determination of emodin and oleanolic acid in Yigankangfuling capsules[J];Chinese Journal of Pharmaceutical Analysis;2008-10
Chinese Journal Full-text Database 1 Hits
1 Cao Hong and Liu Yun(Institute for Drug Control of PLA,Beijing,100071);Determination of Rhein,Emodin,Chrysophanol,Physcion and Aloe-emodin in JinYiNiaoShi Granules and Radix Rhei by HPLC[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;1998-01
Chinese Journal Full-text Database 10 Hits
1 YUAN Yuan 1, CHEN Wan Sheng 1, ZHANG Han Ming 1, CHAI Yi Feng 2, LI Li 1, ZHENG Shui Qing 1 (1.Department of Pharmacognosy, College of Pharmacy, Second Military Medical University, Shanghai 200433, China; 2.Department of Pharmaceutical analysis);Content determination of three kinds of anthraquinones in the root of Rumex by HPLC[J];Academic Journal of Second Military Medical University;2000-10
2 CAO Wei-guo~(1,2),LIU Zhi-qin~1,SHAO Yun~1,TAO Yan-duo~(1*) (1 The Northwest Institute of Plateau Biology,Chinese Academic of Sciences,Xining 810000,China;2 Graduate School of Chinese Academy of Sciences,Beijing 100039,China);Determination of four anthraquinone derivatives in trueborn Rheum tanguticum of Qinghai Province[J];Acta Botanica Boreali-occidentalia Sinica;2004-11
3 JIANG Yun-Gen 1, CHEN Chang-Sheng 2, SONG Yan-Rong 1, FU Long-Gen 1, XIE Wen 1, XU Zhe 1 1Department of Pharmacy, Jiangxi Hospital, Jiangxi Corps of Chinese Armed Police Force, Nanchang 330001, China, 2Department of Health Statistics, School of Preventive Medicine, Fourth Military Medical University , Xi'an 710033, China;Quality standard of Tongluo Quebi Pill[J];Journal of The Fourth Military Medical University;2005-03
4 Wang Geng, Lu Huqing (Guangzhou Junior Medical College of PLA, Guangzhou, 510315);The determination for the content of total anthraquinone of Radix et Rhizoma Rhei in Wei Lin tablets[J];;1999-02
5 Zhang Dan  (School of Pharmacy, Sichuan University, Chengdu 610041) Jiang Xinhui (Department of Pharmacy, Chongqing University of Medical Sciences, Chongqing 400016);Determination of Aloe-emodin, Rhein, Emodin and Chrysophanol in Radix Rhei by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-04
6 ZHOU Jian-bo~1,2,JIANG Fu-quan~1,2,WEN Huai-xiu~1,2, SHAO Yun~1,SHI Zhi-xian~1 and TAO Yan-duo~*1(1.Northwest Institute of Plateau Biology,Chinese Academy of Sciences,Xining 810008;2.Graduate School of Chinese Academy of Sciences,Beijing 100049);Study on HPLC fingerprint of alcohol extracts from Rheum tanguticum[J];Chinese Journal of Analysis Laboratory;2006-11
7 Yao Jia ,Yan Liushui, Luo Guoan (Analysis Center ,Tsinghua University, Beijing, 100084), Yan Chao (You Nite Unimicro Technologies Co, Tongliao, Neimenggu);Design of a capillary electrochromatographic system.[J];Analytical Instrumentation;2001-04
8 YAN Liu-Shui, WANG Zong-Hua, LUO Guo-An *, WANG Yi-Ming(Department of Chemistry, Tsinghua University, Beijing 100084, China);Simultaneous Separation of Five Anthraquinone Compounds inChinese Herb Rhubarb Extracts by Pressurized Gradient Capillary Electrochromatography[J];Chemical Research In Chinese Universities;2004-05
9 ZHENG Zhi-hua 1,ZHU Chen-chen 2 (1.Guangdong Pharmaceutical Association, Guangzhou 510080,China; 2.New Drug Research & Development Center of Guangzhou University, Guangzhou 510405,China);Determination of 5 anthraquinones in rhubarb extracts by HPLC[J];Academic Journal of Guangdong College of Pharmacy;2004-06
10 Zhang Cui,et al Pharmacy College,Harbin University of Commerce,(Heilongjiang Harbin 150076);Determination of Emodin in Qichoutang by HPLC[J];Heilongjiang Medicine Journal;2008-02
Chinese Journal Full-text Database 2 Hits
1 Wang Yuping,Zhu Zhaoyi,Wang Chunlan and Yang Junshan (Institute of Medicinal Plant,Chinese Academy of Medical Sciences ,Peking Union Medical College, Beijing 100094);Determination of Oleanolic Acid and Total Saponins in Aralia L.[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1998-09
2 LIU Xue\|xiang,CHEN Jian\|wei (Nanjing University of Traditional Chinese Medicine,Nanjing 210029);Studies on the Extracting Technique of Oleanolic Acid from Achyranthes bidentata Bl[J];Chinese Journal of Experimental Traditional Medical Formulae;2001-02
【Secondary References】
Chinese Journal Full-text Database 3 Hits
1 QI Dan et al (College of Agronomy,Henan Agricultural University,Zhengzhou,Henan 450002);Effects of Different Sowing Time on the Quantity and Quality of Achyzanthes bidentata[J];Journal of Anhui Agricultural Sciences;2008-28
2 ZHAO Yu-mei1,WANG Jing2,LIANG Sheng-wang1,ZHANG Cui-ying3,FENG Wei-sheng4,ZHZNG Guang-qiang4(1.Guangdong College of Pharmacy,Guangzhou,Guangdong 510006,China;2.Shenyang Pharmaceutical University,Shenyang 110016,China;3.Henan Institute for Food and Drug Control,Zhengzhou 450003,China;4.Traditional Chinese Medicine University of Henan,Zhengzhou 450008,China);Content of oleanolic acid in Radix Achyranthes bidentata before and after storage[J];Journal of Guangdong College of Pharmacy;2008-02
3 CHENG Qi-lai1,LI Hong-liang1,XIONG Mian-li2 (1.Dept. of Pharmacy, Gannan Medical College,Ganzhou 341000,Jiangxi, China; 2.Dept. of Pharmacy, The Municipal Hospital of Ganzhou, Ganzhou 341000, Jiangxi, China);Optimization of the Extraction Technology of Oleanolic Acid from Serissa serissoides by Orthogonal Test[J];Hubei Agricultural Sciences;2009-02
【Secondary Citations】
Chinese Journal Full-text Database 1 Hits
1 Chen Dingyi. Wang Jingzhu and Zhao Xianhong(Beijing University of Traditional Chinese Medicine 100029);Analytical Study on processing of Rheum palmatum L. by HPLC[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1994-09
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved