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《Journal of The Fourth Military Medical University》 2004-07
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Quality standard of Huatengzi Granules

WANG Xiao Juan 1, ZHU Ling Zhen 2, LIU Jie Zhong 1, WANG Rong 1 1Departmeny of Pharmacy, College of Stomatology, 2Institution of Materia Medca, Fourth Military Medical University, Xi’an 710033, China  
AIM: To determine the content of emodin and oleanolic acid in Huatengzi Granules (HTZG) by HPLC. METHODS: ODS C 18 column was used to determine emodin, the methanol and phosphoric acid aqueous solution ratio of the mobile phase being 90∶10 and the methanol water ratio of the mobile phase being 90∶10 in determining oleanolic acid. The detection wave length was 290 nm and 215 nm, respectively. RESULTS: A good linear relationship was obtained between the peak area and the concentration of emodin from 0.1314 to 0.8760 μg ( r =0.9997). The average recovery rate of emodin was 99.56% and RSD was 2.20% . A good linear relationship was obtained between the peak area and the concentration of oleanolic acid from 1.17 to 7.80 μg ( r =0.9998). The average recovery rate of emodin was 100.38% and RSD was l.45%. CONCLUSION: The method employed in this study can be used in quality control of HTZG.
【CateGory Index】: R286.0
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