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Preparation of the complexes of 732 resin with FeCl_3 and their catalysis properties

CHEN Jian fang (Department of Chemistry,Hunan Textlie College,Xiangtan,Hunan 411104,China) CAO Sheng chun (College of Chemistry and Engineering,Hunan University,Changsha 410082,China)  
The supported Fe 3+ 732 resin catalyst was syntheized.Fe 3+ 732 resin has different activity from that of non suppoted 732 resin in this reactions.The influence on activity of catalyst in the reactions of benzene hydroxylation to phenol by exchange method,acid washing and iron content was investigated.As a result,the most favourable one in improving catalytic activity is using acid washing,dynamic exchange method.Optimal phenol yielding rate can reach about 77%.The iron content of catalyst is 79.29 mg per one gram dry resin.
【Fund】: 湖南省科委资助课题!(0 1 942 60 )
【CateGory Index】: TQ426.8
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