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《JOURNAL OF CHONGQING UNIVERSITY(NATURAL SCIENCE EDITION)》 1999-01
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Studies on the Formation Mechanism of SO 2- 4/ZrO 2 Solid Superacid

Zhang Yunhuai Xu Yi Chen Changgou Ou Zhongwen (College of ,Chongqing University)  
The formation of SO 2- 4/ZrO 2 solid superacid is studied with FT IR、XRD and SEM techniques.Subtractive FT IR measurement indicates the existence of chemical bonds between ZrO 2 and H 2SO 4,XRD determination reveals that the strength of SO 2- 4/ZrO 2 superacid strongly depends on temperature of calcination and reaches a maximum as the ZrO 2 transforms into tetragonal crystal phase.SEM analysis shows that the morphology of ZrO 2 surface is changed due to treatment of H 2SO 4.This catalyst shows higher esterification activity for synthesis of dibutyl moleate which is excellently related with the results of surface analysis.
【CateGory Index】: O614.412
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