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《Fujian Journal of Agricultural Sciences》 2006-04
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Determination of propargite residue in vegetables by gas chromatography

GUO Jian-hui~(1),ZHANG Wei-de~(1),CHEN Li-ping~(1),CHEN Yi-nan~(2)(1.Zhangzhou Agricultural Test and Inspection Centre,Zhangzhou,Fujian 363000,China; 2.Food and Biotechnology Department of Zhangzhou Vocational Technical College,Zhangzhou,Fujian 363000,China)  
A method for determining propargite residue in vegetables was established by gas chromatography.The vegetable samples were treated with petroleum ether/acetone(1∶1) or n-hexane/acetone(1∶1),then extracted by agitation,the water-soluble impurities in the extract were removed by liquid-liquid partitioning method,the organic impurities were removed with florisil chromatography,then the detergent of n-hexane/ethyl acetate(95∶5) or n-hexane/acetone(95∶5) was used to elute propargite.Propargite was determined by GC-FPD(with S optical lamella),separated by"Pesticide Residuaes II"capillary column.The results showed that the average recovery of propargite ranged from 88.5%~108.1%,and RSD ranged from 3.14%-9.54%,MDQ was 0.1 ng,LOD was 0.01 mg·kg~(-1) in vegetable samples.This method is simple,accurate,and it can satisfy the analysis of reality samples.
【Fund】: 漳州市科技计划项目(Z03028)
【CateGory Index】: TS255.7
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