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《Fujian Journal of Agricultural Sciences》 2011-05
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Simultaneous Determination of Sulfadiazine and Sulfamethoxazole Residues in Muscle of European Eels (Anguilla anguilla) by HPLC

LIN Li-cong(The Freshwater Fisheries Research Institute of Fujian Province,Fuzhou,Fujian 350002,China)  
A high performance liquid chromatographic method was developed for the simultaneous determination of sulfadiazine and sulfamethoxazole in European eels(Anguilla anguilla) muscle.Homogenized tissue were extracted with 10% sodium sulfate and acetonitrile-Chloroform(10∶1),the extract was concentrated by nitrogen,and redissolved into 2 mL mobile phase and defatted with n-hexane.Sulfadiazine and sulfamethoxazole were separated on Eclipse XDB-C18 Column with mobile phases containing acetonitrile and 0.05 mol·L-1 ammonium dihydrogen phosphate(20∶80) and finally determined by Multiple Wavelength Detector(MWD).The detection limit of sulfadiazine and sulfamethoxazole were 4 μg·kg-1and 8 μg·kg-1.In the range of 0.01~5.0 μg·kg-1,the mean recoveries were more than 80%.The intraday and interday precisions were less than 5%.It showed that the method meet the conventional residue testing requirements.
【Fund】: 福建省科技计划项目——省属公益类科研院所基本科研专项(2010R1001-5)
【CateGory Index】: S859.84
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