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《Non-Metallic Mines》 2008-04
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Study on HCl Doped Polyaniline/Attapulgite Conductive Nanocomposites

Zeng Yongbin1 Yao Chao1 Ding Yonghong1 Li Xiaotang2 Liu Jianping3 (1 Department of Chemical Engineering, Jiangsu Polytechnic University, Changzhou 213164; 2 Jiangsu Engineering Technology Research Center of Attapulgite, Xuyi 211700; 3 Jiangsu NDZ technology Co., Ltd, Changzhou 213016)  
The surface of attapulgite(ATP) was coated with the PANI which doped with Hydrochloric acid to synthesize the HCl-PANI/ATP nanocomposites by in-situ polymerization method. The effects of the polymerization temperature,the covering ratio of aniline,the polymerization time and the amount of Ammonium persulfate(APS) on the volume resistivity were studied. The result indicated that when the covering ratio of aniline was 30%, the polymerization temperature was 20℃, the polymerization time was 4h, the drying time was 2.5h, the molar ratio of HCl, APS and Aniline was 11.63∶1.08∶1, the volume resistivity of nanocomposites could reach to 2.5Ω·cm. And the nanocomposites prepared on this condition was characterized by TG-DTA,XRD and FTIR.
【Fund】: 国家863项目(2007AA06Z118);; 江苏省科技攻关(NoBE2006373、NoBE2006045);; 江苏省博士后基金(No0602020B);; 常州市科技攻关(NoCE2007075)资助项目
【CateGory Index】: TB383.1
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