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《Non-Metallic Mines》 2011-02
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Preparation of O-cresol Formaldehyde Epoxy Resin/Attapulgite Nanocomposites by Melt Polymerization

Ji Qinglin1 Cao Qinghua1 Wang Juhua1 Yu Qiang1 Zhuang Wei1,2,3 Chen Qiang1,2,3(1 School of Material Science and Engineering,Changzhou University,Changzhou 213164;2 High Technology Research Institute of Nanjing University,Changzhou,213164;3 School of Chemistry and Chemical Engineering,Nanjing University,Nanjing 210093)  
Organic-attapulgite(OAT) was obtained by organic modification,and we characterized it by FTIR and XRD.The results showed that the physical adsorption was present in the outer surface of attapulgite crystal rods.Then the ECN/OAT-x(x=1wt% to 5wt%) nanocomposites were respectively prepared by melt polymerization.The nanocomposites were characterized by SEM,DMA,TGA and so on.The results showed that the addition of OAT made the compounds transform from brittle fraction to ductile fracture.The mechanical capability and thermal analysis of the nanocomposies were also measured.In contrast with pure ECN,the tensile strength,impact strength and Tg of ECN/OAT-3 were respectively improved by 54.3%,83.5% and 39.6℃.The thermal stability of nanocomposites was markedly improved.
【Fund】: 常州市工业科技攻关计划(CE20090029)
【CateGory Index】: TB383.1
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