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《Non-Metallic Mines》 2013-04
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Preparation of Polyaniline/Attapulgite/Polysulfone Composite Film Electrode and Their Electrochemical Performance

Suo Longning1 Shang Xiuli1* Wu Haixia1 Tang Rongping1 Zhou Yanqing1 Hu Zhongai2(1 Department of Petrochemical Engineering,Lanzhou Petrochemical College of Vocational Technology,Lanzhou,Gansu 730060;2 Key laboratory of polymer materials of Gansu Province,College of Chemistry and Chemical Engineering,Northwest Normal University,Lanzhou,Gansu 730070)  
Polyaniline/attapulgite(PANI/ATP) conductive nanocomposites doped with hydrochloric acid was prepared by chemical in-situ polymerization.Polymer solution was prepared with PSF as film forming agent,and quantitative adding to the glassy carbon electrode obtained PANI/ATP/PSF composite film electrode.The morphology and structure of sample were characterized by scanning electron microscopy(SEM) and X-ray diffraction(XRD).Capacitance performance of PANI/ATP/PSF composites were investigated by cyclic voltammetry,electrochemical impedance spectroscopy and galvanostatic charging-discharging.These results show that PANI/ATP/PSF composite with porous structure have good capacitance performance in 1 mol/L H2SO4 solution,the specific capacitance reaches 465 F/g at the current density of 0.5A/g.It exhibits lower inter resistance and good cycle stability.
【Fund】: 甘肃省高等学校研究生导师科研项目计划(1015-01);; 甘肃省中青年科技基金(1007RJYA005)
【CateGory Index】: TM53
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