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《Journal of Fujian Medical University》 2006-02
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The Flurimetric Determination of Aloe-emodin and Aloin in Aloe Capsules

Huang Liying, Lai Limin, Chen Wei, Qiu Yinghua, Lin Xinhua Division of Pharmaceutical Analysis, School of Pharmacaceutical Science, Fujian Medical University, Fuzhou 350004  
Objective The flurimetric determination of aloe-emodin and aloin in aloe capsules was described. Methods In the presence of pH 5.6 HAc-NaAc buffer and SDS surfactant, excitation and emission maximal of aloe-emodin were at 460 nm and 550 nm(λex/λem=460/550 nm). Aloin in this system do not emit fluorescence. In the presence of pH 5.6～9.2 NaOH-Na_2B_4O_7 buffer, aloin reacts with borax, the system fluorescence intensity was 10 times that of origin, λ_ ex/λ_ em=387/583 nm. Results The linear range of aloe-emodin was 1.0×10 -6～2.5×10 -5 mol/L in 460/550 nm and aloin was 1.0×10 -6～2.0×10 -5 mol/L in 387/583 nm. Its detection limit was 2×10 -8 mol/L in aloe-emodin and 1×10 -8 mol/L in aloin. Conclusion This method is sensitive, repetitive and simple. It can be applied to the determination of aloe-emodin and aloin in aloe capsules.
【Fund】： 福建省科技厅科研基金资助项目(2002I015)
【CateGory Index】： R286
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