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《Powder Metallurgy Technology》 2010-06
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Study on factors in synthesis of lithium orthosilicates powder by solid state reaction method

Dong Hongying1),Ma Wen2),Zhang Jianyong1),He Xiaodong1),Song Fengyu2)1)(School of Chemical Engineering,Inner Mongolia University of Technology,Hohhot 010051,China)2)(School of Materials Sciences and Engineering,Inner Mongolia University of Technology,Hohhot 010051,China)  
In this research,Li4SiO4 was synthesized with diferent lithium salts and silicon dioxide as starting materials by solid state reaction method.DTA analysis of the different lithium salts shows that Li2CO3 is an optional compound for synthesizing lithium orthosilicates.The formation of lithium orthosilicates at different synthesis temperature and different synthesis time were investigated by TG-DSC,XRD and SEM.Furthermore,the desired phase Li4SiO4 was synthesized after heat treatment at 700℃ for 6hrs.
【Fund】: 内蒙古教育厅资助项目(NJ05051 NJzy08055)
【CateGory Index】: TB383.3
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