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《Radiation Protection》 2012-03
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Study on Preparation of Ultrafine Lead Tungstate for Radiation Protection and γ-ray Shielding of the Gloves

Du Licheng 1,He Ping 1,Zhou Yuanlin 1,Song Kaiping 1,Yang Kuihua 2(1.College of Materials Science and Engineering,Southwest University of Science and Technology,Sichuan Mianyang 621010;2.School of Chemistry and Chemical Engineering,Mianyang Normal University,Sichuan Mianyang 621000)  
Lead tungstate combines the radiation shielding properties of tungsten and lead,and it is quite distinctive to manufacture lead tungstate with ultra-fine granularity to enhance its capacity of radiation shielding.The grain size of lead tungstate has direct impact on the ability of its protection from radioactive materials.the smaller the grain size and more uniform dispersion of lead tungstate,the better protective ability it is going to be.In this paper,soft-template synthesis was introduced to prepare ultra-fine PbWO 4.Rigorous experiment conditions are settled to ensure the access to obtain ultra-fine,homogeneous lead tungstate product,and it is better than other physical and chemical preparation methods.The surface-active agent for the soft template,with S-60 for the water system W/O microemulsion zone,was used to synthesize successfully ultra-fine PbWO 4.It was shown that dispersing agent S-60 in the soft template method produced ultra-fine PbWO 4 with uniform granularity distribution.By using orthogonal experimental method,the best experimental conditions were obtained as follows: S-60 as surfactant dispersant with diluted 30 times concentration,solutions with pH9,0.01 mol/L concentration of reactant,1 300 rpm of stirring speed and slowly adding drops of Na 2 WO 4 solution into Pb(Ac) 2 solution.Based on the optimal experimental conditions,the product of ultra-fine product for the anti-radiation protection filler has been made.The fine packing for the preparation of tungsten the gamma rays on the gloves is an average capacity of 5% or so.
【Fund】: 国防科工委资助课题“高性能射线防护材料研制”(编号:JPPT-115-2-1081)
【CateGory Index】: TL344
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【Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHAI Qing-zhou,LAI Xi (Research Center for Nanotechnology,Changchun University of Science and Technology,Changchun 130022,Jilin,China);A Research on Preparation of Nanometer α-Al_2O_3 Powders[J];Acta Armamentarii;2008-12
2 DIAO Xian-zhen, HOU Chang-jun (Chemistry and Chemical Engineering Department, Chongqing University, Chongqing 400030,China);Preparation of WO_3 Nano-Powder with Microemulsion Methed[J];Chinese Journal of Sensors and Actuators;2006-05
3 SONG Jie CHEN Xiaoming YAN Yuhua (Biomedical Materials and Engineering Center,Wuhan University of Technology,Wuhan 430070);Application of Microemulsion in Preparation of Nanopartieles[J];Materials Review;2003-S1
4 LI Dezeng WU Guangming SHI Jichao WANG Airong SHEN Jun (Pohl Institute of Solid State Physics,Tongji University,Shanghai 200092);Preparation,Applications and Research Trend of Nano-WO_3 Materials[J];Materials Review;2007-S3
5 Wang Maolin1, Wang Xingan1, Yang Zhimao1, Wang Yaping2, Ding Bingjun1 (1. Xi’an Jiaotong University, Xi’an 710049, China) (2. Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China);Preparation of Nanocrystalline La_2O_3 by Sol-Gel Method[J];Rare Metal Materials and Engineering;2005-03
6 Zhou Yuanlin Song Kaiping He Fangfang Du Licheng Xie Changqiong(Key Laboratory for Advanced Building Materials of Sichuan Province,Southwest Scientific and Technical University,Sichuan Mianyang,621010);STUDY AND PREPARATION OF A NOVEL FOAM RUBBER PRODUCT FOR γ-RAY SHIELDING[J];Radiation Protection;2008-01
7 Shi Liyi Hua Bin Zhang Jianping(School of Chemistry, and Chemical Engineering, Shanghai University,Shanghai, 200072,China);Structure of Microemulsion and Application of W/O Microemulsion in the Preparation of Ultrafine Particles[J];JOURNAL OF FUNCTIONAL MATERIALS;1998-02
8 Zhou Liya; Li Chenghai; Gong Fuzhong (College of Chemisitry and Chemical Engineering, Guangxi University, Nanning, 530004);Microemulsion and it's Application[J];JOURNAL OF GUANGXI UNIVERSITY;1999-S1
9 PAN Hai-min,YANG Bo-lun~*,LI Guo-zhi,HE Yong-jun (Department of Chemical Engineering, Xi'an Jiaotong University, Shanxi Xi'an 710049, China);W/O Micro Emulsion Technology and the Controlled Synthesis of Nanoparticles[J];Huaxue Shijie (Chemical World);2005-01
10 SHAO Ming CHEN HongFang LI Cheng CHEN Hui XU ZiZong WANG ZhaoMin (Department of Modern Physics, University of Science and Technology of China, Hefei 230026, China);Testing the Radiation Hardness of Lead Tungstate Scintilating Crystals[J];HIGH ENERGH PHYSICS AND NUCLEAR PHYSICS;2000-06
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 Li Da cheng,Zhou Da li,Liu Heng,Zhang Ping,Zhang Yun (Institute of UFP materials,Sichuan University(west),Chengdu 610065,China) Gong Jia zhu (Sichuan Longmang Titanium Industry Co.,Ltd,Mianzhu 618200,China);The Characters of Nanometre TiO_2[J];Sichuan Nonferrous Metals;2002-03
2 REN Cheng-jun~1,3 ,LI Da-cheng2,ZHONG Ben-he1,ZHOU Da-li2,LIU Heng2,GONG Jia-zhu4 (1.Chemical Engineering College Sichuan University,Chengdu 610065) (2.Material College Sichuan University,Chengdu 610065) (3.The Faculty of Chemistry Sichuan University,Chengdu 610064) (4.Sichuan Longmon Titanium Industry Co.Ltd,Mianzhu City 618200);Factors affecting photo catalytic activity of TiO_2 and measures improving its potocatalytic performance[J];Sichuan Nonferrous Metals;2004-04
3 Qian Yiqing, Zhao Ping, Wang Weihua (College of Materials Science and Engineering, Nanjing University of Chemical Technology 210009);PREPARATION AND ANALYSIS OF EMULSION POLYMER OF ALKYLABLE NANO-SiO_2/MMA AND ITS MODIFYING EFFICIENCY TO PC[J];Engineering Plastics Application;2002-01
4 Wang Xiaojun (College of Polymer Material Science & Engineering, Sichuan University, Chengdu 610065, China)Yang Jie, Long Shengru (Institute of Materials Science & Technology, Sichuan University, Chengdu 610064, China);NANOMATERIAL AND ITS APPLICATION IN THE MODIFICATION OF THE ENGINEERING PLASTICS[J];Engineering Plastics Application;2002-10
5 Liu Jianlin, Xiao Jiumei, Shi Xiaoqun, Gong Chunxiu, Ma Wenjiang (College of Applied Science in University of Science and Technology Beijing, Beijing 100083, China);STUDY ON THE DISPERSION AND MECHANICAL PROPERTIES OF NANO-CaCO_3 FILLED EPOXY RESIN[J];Engineering Plastics Application;2003-03
6 Hui Xuemei, Zhang Wei, Wang Xiaojie (The 43rd Institute of the Fourth Academy of CASC, Xi' an 710025, China);STUDY ON THE PROPERTIES OF EPOXY/SiO_2 NANO-COMPOSITES[J];Engineering Plastics Application;2004-02
7 An Jun, Wu Haixia, Xin Yinchang (College of Chemical Engineering and Material Scince, Shandong Normal University, Jinan 250014, China);PREPARATION AND RESEARCH OF RESIN/NANO-LEAD COMPOSITE FOR HIGH-ENERGY RADIATION PROTECTION[J];Engineering Plastics Application;2004-12
8 Zheng Haizhong~(1,2),Zhang Jian~(1),Lu Shiqiang~(1,2), Xu Zhifeng~(1)(1.Nanchang Institute of Aeronautical Technology,Nanchang 330034,China;2.Nanjing University of Aeronautics & Astronautic,Nanjing 210016,China);PREPARATION OF PS/Al_2O_3 NANOCOMPOSITE BY SELECTIVE LASER SINTERING[J];Engineering Plastics Application;2005-09
9 An Jun, Liu Jihua, Xin Yinchang (College of Chemistry, Chemical Engineering and Material Science, Shan Dong Normal University, Jinan 250014, China);PREPARATION OF RESIN NANO-CERIUM SHIELDING RADIATION COMPOSITE AND ITS PROPERTIES RESEARCHING[J];Engineering Plastics Application;2006-08
10 XU Ling1,LIU Chang-ling2,XU Hai-Yan1,WU Shi-biao1,WANG Feng1,LI Chun-yan2(1.School of Materials & Chemical Engineering,Anhui University of Architecture,Hefei 230022,China; 2.Department of Chemistry and Chemical Engineering,Hefei Normal University,Hefei 230061,China);Cooperative Photocatalytic Degradation of Methyl Orange by H_2O_2 and CuO Thin Film[J];Journal of Hefei Normal University;2012-03
China Proceedings of conference Full-text Database 10 Hits
1 Liu Yajin, Liang Xiaoping , Jiang Qiang, Li Wandeng (Tianjin Municipal Key Lab of Fiber Modification and Functional Fiber, Tianjin Polytechnic University, Tianjin 300160, China);Preparation and Evaluation of Nanoscale ZnO Anti-UV Agents[A];[C];2005
2 ;Preparation and Application of Nanoseter Silica[A];[C];2008
3 CHENG You-gang,LIU Yan,ZHANG Guo-bing (Yancheng College of Textile Technology Jiangsu,Yancheng 224001);Study on the antibacterial performance & anti-UV radiation of silk fabric treated with nano-ZnO[A];[C];2011
4 CHENG You-gang,LIU Yan (Yancheng College of Textile Technology Jiangsu,Yancheng 224001);Research on modified dispersion of Nanometer zinc oxide[A];[C];2011
5 HAO Chuncheng XIAO Feng YUAN Shenli (College of Materials Science and Engineering,Qingdao University of Science and Technology,Qingdao 266042);Preparation of Nanometer Copper in Inverse Microemulsions[A];[C];2007
6 Wang Quanjie1,2,3,Qin Xuefei1,Wang Qianqian1,Wang Yanqing3(1.Chemistry and Biology College,Yantai University,Yantai 264005,China;2.State Research and Promotion Center of Leather Making Technology,Yantai 264003 China;3.College of Resource and Environment,Shaanxi University of Science and Technology,Xi’an 710021,China);Research Progress of Application and Uniform Dispersion on Carbon Nanotubes[A];[C];2010
7 LEI Ting;LOU Feng-lan;TANG Guang-ming;BO Xin-wei Chongqing Instrument Materials Research Institute, Chongqing, 400700, China;Synthesis of the Nickel Ferrite Nano Powder by Hydrothermally Method[A];[C];2001
8 YAO Lan-fang, ZHU Yong-an, YUE Chun-xiao (Department of Physics, Science College, University of Shanghai for Science & Technology, Shanghai 200093, China);Application of nano-materials in stealthy technology[A];[C];2006
9 WANG Sheng-hao, WEN Feng, HAO Wan-jun, CAO Yang (The Key Laboratory of Tropical Biological Resources of Chinese Education Ministry, Department of Materials Science, School of Science & Engineering, Hainan University, Haikou 570228, China);The research status and prospect of nano-radar stealth materials[A];[C];2006
10 ZHANG Yan-hua, LIYing-lan, TU Hong-qing, MENG Xiang-min (Department of Physics, Beijing Institute of Technology, Beijing 100081, China; Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100101, China);Synthesis and infrared absorbing properties of Ag/Zn/Ag nanoparticles film[A];[C];2006
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Jiang Pingping, Shen Fenglei, Yang Chunling, Yin Fushan (Wuxi University of Light Industry 214036);THE STUDY STATUS AND DEVELOPING TREND OF ANTIRADIATION PMMA[J];Engineering Plastics Application;1999-01
2 HE Ke-lan,LIN Jian,QIN Shuang (School of Materials Science and Engineering,Tongji University,Shanghai 200092,China);Development of Preparation and Application of Alumina Nanopowder[J];Glass & Enamel;2006-05
3 DIAO Xian-zhen, HOU Chang-jun (Chemistry and Chemical Engineering Department, Chongqing University, Chongqing 400030,China);Preparation of WO_3 Nano-Powder with Microemulsion Methed[J];Chinese Journal of Sensors and Actuators;2006-05
4 HUANG Shi-zheng, LIN Wei, CHEN Wei, CHEN Zhi-qian (Inst. of Gas Sensing Sensor, Fuzhou University,Fuzhou 350002,China);Study on H_2S gas sensor of WO_3-ZnS nanosized material[J];Journal of Transducer Technology;2001-01
5 Liang Zongcun Shen Hui (Guangzhou institute of energy conversion,CAS,Guangzhou 510070);Preparation and Current Status of Nano WO_3 Thin Films[J];Materials Review;2000-03
6 LI Xiaofang ZHANG Yali SUN Dianting (College of Chemical Engineering, Qingdao University, Qingdao 266071);Nano-WO_3 Film[J];Materials Review;2003-S1
7 SONG Tao,QIU Tai,SHEN Chun-ying,LI Zhi-shun,CHEN Xiao-jie(College of Materials Science and Engineering,Nanjing University of Technology, Nanjing 210009,China);Preparation of Ultrafine Plate-like WO_3 via W/O Microemulsions Method[J];Journal of Materials Science and Engineering;2007-01
8 Wang Jinshu, Zhou Meiling, Zhang Jiuxing, Nie Zuoren, Zuo Tieyong (Beijing Polytechnic University, Beijing 100022);High Temperature XPS Study of Carburized La_2O_3-Mo Cathode Material[J];RARE METAL MATERIALS AND ENGINEERING;2000-04
9 Dong Xiangting 1,Liu Guixia 1, Sun Jing 1, Li Jianli 1, Liu Jinghe 1,Hong Guangyan 2 (1 Changchun Institute of Optics and Fine Mechanics,Changchun 130022) (2 Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022);Preparation and Properties of Nanocrystalline Yb_2O_3[J];Rare Metal Materials and Engineering;2001-01
10 TANG Yi-ke1 XU Yan1 XU Jing1 WEI Li-Fan2 (1. The State Key Laboratory of Mechanical Transmission, Chongqing University, Chongqing 400044; 2. China Academy of Engineering physics, Mianyang 621000);Current Status and Developmental Trend of Preparation of WO_3 Thin-film[J];;2005-01
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