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《China Powder Science and Technology》 2008-04
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Synthesis and Characterization of Silver Nano-particles in Interlamellar Space of Kaolinite Composites

Du Yitinga,b, Wang Linjianga,b, Xie Xianglib (a.Key Laboratory of Nonferrous Materials and New Processing Technology, Ministry of Education; b. Department of Materials and Chemistry Engineering. Guilin Univerisity of Techology, Guilin 541004 China)  
Useing the kaolinite-dimethyl sulfoxide (DMSO) to be the precursor, then it was substituted by silver nitrate in the interlamination of kaolinite.The kaolinite interlamination was used as a reactor to control the silver particle size.The reductant hydrazine hydrate was used to reduce sliver for preparing kaolinite-sliver intercalation complexe. Then the intercalation complexe was charactered by infrared spectrum, it was seen that the intercalation performance destructed the interlayer hydrogen bond. DMSO formed the hydrogen bond with inner surface hydroxyl groups of kaolinite. Inserting of silver made the sharp diffraction peak of the Ag(111)at 2θ=38.110 8~38.394 2°. TEM characterization indicated that the silver had already intercalated into the layers of kaolinite,but the particle size distributed nonuniformity.
【Fund】: 国家自然科学基金项目 编号:40672026
【CateGory Index】: O611.3
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