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《Acta Materiae Compositae Sinica》 2006-06
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Non-isothermal crystallization behavior of nano-CaCO_(3)/PP composites modified by macromolecular compatibilizers

WANG Yuhai,SHEN Hao,MAI Kancheng~*(Key Laboratory for Polymeric Composites and Functional Materials of Ministry of Education,Materials Science Institute, College of Chemistry and Chemical Engineering,Zhongshan(SUN Yat-sen) University,Guangzhou510275,China)  
The nano-CaCO_(3)/PP composites modified by four kinds of compatibilizers were prepared respectively.The crystallization and melting behavior of PPbase composites were investigated using DSC and WXRD.The(results) indicate that the addition of nano-CaCO_(3) increases the crystallization temperature of PP and induces the formation of β-PP crystal due to the heterogeneous nucleation of nano-CaCO_(3).The heterogeneous nucleation of PP-g-AA and PP-g-MA is also observed for PP crystallization.The synergism of heterogeneous nucleation of nano-CaCO_(3) and PP-g-AA(PP-g-MA or POE-g-MA) further increases the crystallization and melting temperatures of nano-CaCO_(3)/PP composites.Addition of PP-g-MA and POE-g-MA induces the formation of more β-PP crystal in nano-CaCO_(3)/PP composites.However,addition of EVA-g-MA decreases the heterogeneous nucleation of nano-CaCO_3.The results suggest that the heterogeneous nucleation of PP in nano-CaCO_(3)/PP composites depends on the inter-(facial) interaction between nano-CaCO_(3)and PP,which is influenced by compatibilizers.
【Fund】: 国家自然科学基金(50573094);; 高等学校博士学科点专项科研基金;; 广东省自然科学重点项目(021731);; 广州市科技局项目(2005Z3D2131)
【CateGory Index】: TB383.1
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