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《ANALYSIS AND TESTING TECHNOLOGY AND INSTRUMENTS》 1998-04
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? Catalytic Spectrophotometric Determination of Trace Amount of Manganese by Potassium Periodate-Fuchsin Acid-Nitrilo Triaceticacid-Dodecyl Dimethylamino Acid System

Xie Zenghong Lian Ronghua Fu Yanbin Zheng Zhaosheng (Department of Chemistry, Fuzhou University Fuzhou 350002)  
A new catalytic spectrophotometric method for the determination of trace amount of Mn(∏) has been developed. The method is based on the oxidation of fuchsin acid with potassium periodate in the presence of nitrilo triaceticacid as an activator and dodecyl dimethylamino acetic acid (DDMAA) as a sensitizer. The sensitivity is increased by 7 times(the rage 1.2~ 2.4 μg/L) and 14 times(the rage 2.4~5.2 μg/L) than that in the absence of the DDMAA. The relative standard deviation was 2.0% for 4.0 μg/L Mn(∏)(11 replicates). The limit of detection for Mn is 1.4~10 -10 mg/L. The method has been succesfully applied to the determination of Mn in tea sample.
【Fund】: 福建省自然科学基金
【CateGory Index】: O614.711,O657.32
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