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《Chinese Journal of Analytical Chemistry》 1989-07
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STUDY ON KINETIC ANALYSIS Ⅴ.CATALYTIC COLORIMETRIC DETERMINATION OF TRACE VANADIUM

Xue Fenghe Zhang Zhiqi Chen Li (Department of Chemistry,Shaanxi Normal University,Xi′an)  
A simple and sensitive catalytic colorimetry has been developed for determination of trace vanadium. It is based on the catalysis of V (V) to decoloration of safranine O oxidized with potassium bromate in diluted sulfuric acid medium in the presence of ascorbic acid. The linear range of determination is 0.005—10μg/25ml V(V). The sensitivity is 8×10~(-12) g/ml. Combining with separation of ionic exchange, the method has been applied to the determination of trace vanadium in natural water and human hair. The mechanism of reaction is investigated, too.
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