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《Chinese Journal of Analytical Chemistry》 1991-11
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Determination of Arsenic,Antimony and Bismuth by Inductively Coupled Plasma-Atomic Emission Spectrometry With Flow Injection Analysis and Hydride Generation

Gao Hanshan Li Kedong (Research Institute of Geology for Mineral Resources,CNNC,Guilin 541004)  
A method for the determination of As,Sb and Bi is proposed by using ICP-AES, flow injection analysis(FIA)and hydride generation.Sample are dissolved in aqua regia, and passed through sampling system of FIA with 10% KI-5% ascorbic acid-5% thiourea solutim as interfrence-free agent.Having continueonsly sampled with constant time and volume,their hydrides have been separated by gas-separator into ICP-AES,and determined The detection limit of As,Sb and Bi was 0.2,0.2 and 0.1μ/g,the range of determination was 0.2~1000μg As/g,0.20~300μg Sb/g and 0.1~300μg Bi/g,respectively,and the analy- sis rate is 60 sample/h.The method was fast and sensitive.
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