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《Chinese Journal of Analytical Chemistry》 1992-11
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Determination of Microamount of Zinc(Ⅱ) in Water by New Reagent 1,3-Bis(4-phenylazophenyl)triazene

Zhu Yurui~*, Jiang Wanquan, Deng Changping, Jin Gu(Deparment of Applied Chemistry, University of Science and Technology of China, Hefei 230026)  
A sensitive reaction of Zn(Ⅱ) with a new reagent 1, 3-bis(4-phenylazophenyl) triaezne [4,4′-Biazobenzenediazoaminoazobenzene(BBDAB)] in the presence of borax and Triton X-100 is presented. The apparent molar absorptivity of red complex has been measured to be 1.63×10~5 L·mol~(-1)·cm~(-1) at 525nm. The calibration curve is linear over the range of 0~8μg/25ml. The molar ratio of Zn (Ⅱ) to BBDAB in the complex is estimated to be 1: 2. Most metal ions do not interfere. The recommended procedure was applied to the determination of Zn(Ⅱ) in waste water sample with satisfactory results.
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