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《Chinese Journal of Analytieal Chemistry》 1996-06
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Determination of Mercury (Ⅱ) by Flow Injection Chemiluminescence Analysis With Inorganic Coupling Reaction─K_4Fe (CN)_6-Luminol system

Zhao Zhiqiang; Wang Zhikui; Jia Yujiang; Zhang Zhujun(Department of chemistry, Shanxi Normal University, Xi'an 710062)  
A flow injection chemiluminescence(CL) analysis with inorganic coupling reaction is developed for the determination of trace mercury(Ⅱ), using the accelerating effect of mercury on the decomposition of K4Fe (CN)6.The detection limit of the method is 2.2 ×10-7 g/L. CL intensity is linearly related to the mercury concentration in thc range of 0. 8~40μg/L. The relative standard deviation is 3. 4% for 8 μg/L Hg. The method has been used for the determination of trace mercury in the environmental water samples with satisfactory results.
【CateGory Index】: O657.32
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