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《Chinese Journal of Analytieal Chemistry》 1996-11
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High-Performance Liquid Chromatographic Analysis of Catechol Product

Deng Guocai; Xu Li; Liu Xinying;Mu Ruicai;Liu Zhi;Gao Li; Ma Hongtao; Li Qinggang; Liu Jingjiang; Chen Rongti(Department of Chemistry, Nankai University, Tianjn 300071)  
This paper reports the analysis of catechol product by HPLC using a silicagel column. With hexane-isopropanol-acetic acid as mobile phase and by gradient elution method,the o-, m-, p- dihydroxybenzene isomers, phenol and p-benzoquinone can be separated fairlywell- The recovery of catechol is higher than 98%, the relative standard deviation is lessthan 0. 2%, and the detection limit of impurities is 10 mg/L.
【CateGory Index】: O657.7
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