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《Chinese Journal of Analytieal Chemistry》 1997-03
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Flow Injection Analysis/Chemiluminescence Detection of Trace Hydrazine in Air

Wu Yuanyuan, Zhao Fang, Geng Zheng, Chen Zhanguo, Liu Qianguang (Department of Chemistry, Shaanxi Normal University, Xi'an 710062)  
A new analytical method consisting of flow injection sampling and chemilumi- nescence detection for determination of trace hydrazine is described. It is based on the ab- sorption of hydrazine in air by 2.0 mol/L H2SO4 and the chemiluminescence reaction of lumi- nol-KIO4-N2H4 system. The linearity of the chemiluminescence intensity holds for the con- centration range of 1.0×10-81.0×l0-6g/mL hydrazine. The detection limit of hydrazine is 4×10-9 g/mL. The relative standard deviation is less than 3% with a sampling rate of 80 samples per hour. The method has been applied to the determination of trace hydrazine in air with satisfactory results. The method is simple, rapid, sensitive and selective. The lowest detectable content of hydrazine is 0.002 mg/m3 in l20 L air sample.
【CateGory Index】: O657.3
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