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《Chinese Journal of Analytieal Chemistry》 1997-03
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Flow Injection Analysis/Chemiluminescence Detection of Trace Hydrazine in Air

Wu Yuanyuan, Zhao Fang, Geng Zheng, Chen Zhanguo, Liu Qianguang (Department of Chemistry, Shaanxi Normal University, Xi'an 710062)  
A new analytical method consisting of flow injection sampling and chemilumi- nescence detection for determination of trace hydrazine is described. It is based on the ab- sorption of hydrazine in air by 2.0 mol/L H2SO4 and the chemiluminescence reaction of lumi- nol-KIO4-N2H4 system. The linearity of the chemiluminescence intensity holds for the con- centration range of 1.0×10-81.0×l0-6g/mL hydrazine. The detection limit of hydrazine is 4×10-9 g/mL. The relative standard deviation is less than 3% with a sampling rate of 80 samples per hour. The method has been applied to the determination of trace hydrazine in air with satisfactory results. The method is simple, rapid, sensitive and selective. The lowest detectable content of hydrazine is 0.002 mg/m3 in l20 L air sample.
【CateGory Index】: O657.3
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Chinese Journal Full-text Database 10 Hits
1 Du Lingyun, Wang Shuhao, Zhang Aimei (Department of Chemistry, Uaocheng Teachers College, Liaocheng 252059);Determination of Hydrazine Using the Inhibitory Effect of Hydrazine on the Reaction of Neutral Red with Nitrite[J];Chinese Journal of Analytical Chemistry;1999-08
2 Qu Wanyun~(1,2),Wang Hong~1,Wu Kangbing~(*1)()~1(Department of Chemistry,Huazhong University of Science and Technology,Wuhan 430074)()~2(Department of Chemistry,Hubei Institute for Nationalities,Enshi 445000);Electrochemical Behavior and Determination of Isoniazid at Multi-wall Carbon Nanotube Modified Electrode[J];Chinese Journal of Analytical Chemistry;2005-10
3 WANG Yang, FAN Shi-hua~*(Research Center for Analysis Sciences, Scientific College, Northeastern University, Shenyang110004);Applications and Progress in Analysis of Atmosphere Pollutants by Chemiluminescence[J];Journal of Analytical Science;2005-02
4 LiXiaoyan,HeZhike , ZengYun (DepartmentofChemistry,WuhanUniversity,Wuhan,430072);Application of ChemiluminescenceinEnvironmentalAnalysis[J];JOURNAL OF ANALYTICAL SCIENCE;1999-03
5 LIU Yan ling 1, FENG Ai xia 2, FAN Dong mei 1 (1. Dept. of Chemistry, Luliang Teachers′ College, Luliang 033000, China; 2. Dept. of Chemistry, Shanxi University, Taiyuan 030006, China);PROGRESS OF APPLICATION OF FI-CHEMILUMINESCENCE TO THE DETERMINATION OF PHARMACEUTICALS[J];Physical Testing and Chemical Analysis Part B Chemical Analysis;2005-04
6 MA Li~ 1,2 , ZHANG Xin-Shen~2, MIAO Pei-Kai~2 (1. Department of Environment Engineering , College of Architecture and Environment, SiChuan University , Chengdu,610065, China;2.Key Laboratory of Leather Chemistry and Engineering (Sichuan University),Ministry of Education,Chengdu 610065,China);Applications and Developments of Flow Injection Analysis in Environmental Monitoring[J];Leather Science and Engineering;2005-03
7 PENG You yuan (Dept. of Chem.,Quanzhou Normal College,Fujian 362000,China);Flow Injection Chemiluminescence Analysis[J];Journal of Quanzhou Normal College;2002-06
8 ZHAO Rut; LIU Xiao-jun; ZHANG Xiu-qi; WU Ya-yan (Institute of Analytical Science,Northwest University, Xi'an 710069, China);Automated on-line monitoring hydrazine in boiler feed water of power plants[J];;1999-06
9 Wu Fuli Zhang Guangyou Yan Xi Hu Wenxiang(1 Institue of Military Medicine, Department of Logistics,Department of General Equipment, Beijing, 100101) (2 Department of Chemistry, Beijing Normal University, Beijing, 100875);Advance in the Research of the Analysis and Detection Technology of Hydrazines Propellant[J];Modern Instruments;2001-06
10 WU Yuan-yuan (Biology and Chemistry Department,Xingtai Senior Teacher's College,Xingtai,Hebei,054001);Study on the Effect of Semicarbazide on Chemiluminescence During the Qxidation of Luminol with Periodate[J];Journal of Xingtai Senior Teachers College;2000-04
Chinese Journal Full-text Database 2 Hits
1 Geng Zheng, Zhang Zhiqi, Bian Lujiao (Department of Chemistry, Shaanxi Normal University, Xi'an);Study on the Determination of Trace Manganese by Luminol-Mn(Ⅱ)-KIO_4 Ghemiluminescence System[J];Chemical Research In Chinese Universities;1988-11
2 Sun Hong et al.(Benxi Municipal station of Environ.Monitoring,Benxi 117021);Study on the Spectrophotomehic pDlimethylaminobenzaldehyde in water.[J];CHINESE JOURNAL OF ENVIROMENTAL SCIENCE;1995-01
Chinese Journal Full-text Database 10 Hits
2 Yang Guangsong (Department of Chemistry);The Geometry of AX_n Species[J];Journal of Anhui Normal University(Natural Science);1990-01
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4 Wu Wanwei Tian Hongjian (Department of Chemistry);FUNCTIONS OF BORIC ACID IN NICKEL PLATING SOLUTION[J];Journal of Beijing Normal University(Natural Science);1989-02
5 SHAO Hua-yue (Dept.of Biologic and Chemical Engineering,Chaoyang Normal College,Cha oyang,Liaoning,122000,China);A Comparison between Lithium bond and Hydrogen bond[J];Journal of Benxi College of Metallurgy;2003-02
6 Zhang Shiguo;The Molecular Mechanics Study for the Conformation and Stability of the 18—crown—6 and Its Aikali Ions Complexes[J];;1992-04
7 WANG Min CHU Xian-ping CHENG Le-hua(Department of Chemistry,Chaohu College,Chaohu Anhui 238000);APPLICATION OF RARE EARTH β-DIKETONE COMPLEX[J];Chaohu College Journal;2006-06
8 Lou Qizheng(Dept. of Biology and Chemistry,Jinhua Educational College,Jinhua, 321000);Some Problems in Inorganic Chemistry Teaching[J];Journal of Chongqing Teachers College(Natural Science Edition);1999-S1
9 CHEN Yong-hua(Department of Chemistry and Environment Engineering,Changsha University of Science and Technology,Changsha 410077,Hunan,China);Influence of Material Structures and Other Factors on the Mechanisms of Inorganic Reaction[J];Journal of Changsha University of Electric Power(Natural Science);2005-04
10 Su Zhongmin Cui Ruihai Fang Zhuiwen Li Jinchang Sheng Lianxi (Department of Chemistry,Northeast Normal University,Changchun);Quantum Chemistry Study of the Intramolecular Hydrogen and Lithium-bonding of Symmetry Organic Molecules[J];Journal of Northeast Normal University;1993-03
China Proceedings of conference Full-text Database 1 Hits
1 Zhang wei~1 Cheng Danhong~2 Yu Zuzhan~3 Werner Jillek~4 1.Dept.of Chemistry of College of Science of Shanghai University,Shanghai 200444; 2.Dept.of Students of China Executive Leadership Academy Pudong,Shanghai 201204; 3.Dept.of Chemistry of Fudan University,Shanghai 200433; 4.Dept.of EFI of Georg-Simon-Ohm-Fachhochschule,Nürnberg 90489,Germang);Electrochemical Migration of SnAgCu Solder Joints on PCB[A];[C];2007
Chinese Journal Full-text Database 10 Hits
1 Yang Jidong (Fuling Normal College,Chongqing 408003);Determination of Hydrazine Anhydrous by Flow-Injection Analysis with Chemiluminescence Detection[J];Chongqing Environmental Science;2002-03
2 Gao Qi 1, Dou Xianmin 2(1.Collage of Basic Science,Henan Agricultural University;Zhengzhou 450002;2.Zhengzhou Institute of Light Industry,Zhengzhou 450002);Determination of Trace Nitrite in Water Samples of the Environment Using Cheniluminescence[J];Chongqing Environmental Science;2003-04
3 Ma Chunlian,Yuan Yingxian,Li Lianshan (Pingdingshan Institute of Technology,pingdingshan 467001);Formaldehyde Optimal Trial Condition with Acetyl Acetone Spectrophotometer[J];Chongqing Environmental Science;2003-08
4 Zhu Xiuhui,Yu Zhen′an;The Study of Alizarin Violet OP H 2O 2 Ti(Ⅳ) Chemiluminescence System[J];JOURNAL OF NORTHEASTERN UNIVERSITY;1997-03
5 Lu Xiaohu Lu Minggang Chen Bing Zhao Guiwen(Department of Applied Chemistry, University of Science and Technology of China, Hefei 230026);STUDY ON THE OXIDIZATION CHEMILUMINESCENCE OF LUCIGENIN SYSTEM SENSITIZED BY ACETONE AND ITS APPLICATION[J];Chinese Journal of Luminescence;1992-03
6 Li Shaoqing; Du Xiaoren; Chen Ying(Department of Applied Chemistry, Xi'an College of Geology, Xi'an 710054);CHEMILUMINESCENCE OF LUMINOL-KIO_4-Co(1, 10-phen·)_3 ̄(2+) SYSTEM AND ITS APPLICATION[J];CHINESE JOURNAL OF LUMINESCENCE;1996-01
7 YANG Ji-dong;Application of Chemiluminescence Analysis in the Environmental Analysis and the Pharmaceutical Analysis[J];Journal of Fuling Teachers College;2001-04
8 XIE Cheng gen(Department of Chemistry,Wanxi College,Lu′an 237012);Flow Injection Analysis of Tyrosine withEnhanced Chemiluminescent Detection[J];Journal of Huaibei Industry Teachers College (Natural Sciences Edition);2002-02
9 YANG Bao-jun~1,CHEN Jian-ping~2,JIAO Tian-shu~2,LI Zhi-kun~2,LIANG Kai-lun~2,LU Gong-xuan~1 (1.State Key Laboratory for Oxo Synthesis and Selective Oxidation,Lanzhou Institute of Chemical Physics,CAS,Lanzhou 730000,China;2.China Jiuquan Satellite Launch Center,Jiuquan 732750,China);Improved Analytical Method for Determining the Purity of Unsymmetrical Dimethylhydrazine[J];Analysis and Testing Technology and Instruments;2006-04
10 An Jingru, Lin Jinming (Department of Chemisttry, Fuzhou University, Fuzhou, 350002);Investigation of Electrochemiluminescence of New Reagent 5-(p-Aminophenylazo)-2,3-dihydro-1,4-phthalazine-1,4-dione[J];Chinese Journal of Analytical Chemistry;1991-03
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 MA Guixia1, ZHANG Tonglai1, ZHANG Jianguo1, MIAO Yanling1, YU KaiBei2(Beijing Institute of Technology, Beijing100081, China);Molecular Structure and Thermal Decomposition Mechanism of Semicarbazide Hydrochloride[J];Chinese Journal of Explosives & Propellants;2003-02
2 WU Yan\+1,LIU Qing\+1,HU Ke\+1,XU Wei hong\+2 (1.Chengdu Institute of Biology,The Chinese Academy of Sciences, Chengdu 610041, China;2 Sichuan Jiufeng Natural Medicine Co.,Ltd,Maoxian 623200, China);PRESENT STATUS OF TAXUS RESOURCES AND INDUSTRIAL DEVELEPMENTSTRATEGIES OF TAXOL IN CHINA[J];Resources and Environment in the Yangtze Basin;2002-06
3 Li Chunxiang~(*),Zeng Yunlong(Chemistry and Chemical Engineering College,Hu′nan University of Science and Technology,Xiangtan 411201);Electrocatalytic Behavior of Poly(2,6-pyridinedicarboxlic acid)/Multi-walled Carbon Nanotube Modified Electrode[J];Chinese Journal of Analytical Chemistry;2006-07
4 WANG Yang, FAN Shi-hua~*(Research Center for Analysis Sciences, Scientific College, Northeastern University, Shenyang110004);Applications and Progress in Analysis of Atmosphere Pollutants by Chemiluminescence[J];Journal of Analytical Science;2005-02
5 CAI Ru xiu, HE Zhi ke and LIU Zhi hong (Department of Chemistry, Wuhan University, Wuhan 430072);Photometric analysis[J];Analytical Laboratory;2001-05
6 Yang-Qiong Zhou Dan-dan (College of Chemistry and Chemical Engineering,Baoji University of Arts and Sciences,Shaanxi Baoji 721000);Study on Synthesis of a Medicine Intermediate-Acetone Semicarbazone[J];Guizhou Chemical Industry;2007-06
7 ZHANG Yang,et al.(Life Science and Geography College of Qinghai Normal University,Xining,Qinghai,810008,China);Effect of 2,4-D and 6-BA on Callus Induction from Rheum Tanguticum[J];Journal of Henan Institute of Science and Technology(Natural Sciences Edition);2006-02
8 QUAN Xin-jun1,MAN Wen-hui2,SONG Nai-zhong1,ZHENG Song-zhi1,WANG Hong-yan1,JIN Wei-qun1(1.College of Chemistry,Jilin University,Changchun 130012,China;2.College of Bio-Scientific and Technical,Changchun University,Changchun 130022,China);Determination of Ceftriaxone Sodium by Flow Injection Chemiluminescence[J];Journal of Jilin University(Science Edition);2008-06
9 XIONG Yang-hui,HU Yong-gang,PANG Zhi-tao(Institute of Environmental Science and Engineering,Huazhong University of Science and Technology,Wuhan 430074,China);FIA-Chemiluminescence Determination of Protein[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2008-03
10 LUO Meng-jiao1,ZHANG Xin-shen1,JIAN Tie-zhu2, LI Wei1,ZHANG Yi2,HU Wei2,XIE Yong-hong1 (1.Key Laboratory of Leather Chemistry and Engineering (Sichuan University), Ministry of Education, Chengdu 610065,China;2.College of Light & Textile and Food Industry, Sichuan University , Chengdu 610065, China);Determination of Water Chroma by FIA-Spectrophotometry[J];Leather Science and Engineering;2007-06
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