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《Chinese Journal of Analytieal Chemistry》 1998-02
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Determination of Trace Iron by Extraction Catalytic Kinetic Spectrophotometry

Sun Dengming, Liu Junying, Yuan Dawen (Department of Chemistry, Huaibei Coal Normal College, Huaibei 235000)  
A new extraction catalytic kinetic spectrophotometric method for the determina- tion of trace iron is studied. The method is based on the iron(Ⅲ ) catalyzed oxidation of o- aminophenol by hydrogen peroxide in weak acidic medium at pH 5. 5. The reaction time, concentration of o-aminophenol in aqueous phase and degree of reaction are controlled by ex- traction equilibrium. The absorbance of organic phase is measured at 424 nm. The linear range of the determination is 0. 50-40μg/L. The detection limit is 1. 6 ×10-7 g/L. The method has been applied to the determination of trace iron in water, human hair and food samples with satisfactory results.
【Fund】: 煤炭青年科学基金;; 安徽省高等学校自然科学基金资助课题
【CateGory Index】: O657.3
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