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《Chinese Journal of Analytieal Chemistry》 1998-08
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Polarographic Adsorption Wave of Vanadium (Ⅴ)-Bathophenanthroline Complex

Zhou Changli (Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000) Lu Yan, Li Xiuling, Cao Wei, Zhao Yingchun (Department of Applied Chemistry, Shandong Institute of Building Materials, Jinan 250022)  
The polarographic behavior of Vanadium(Ⅴ)4,7-diphenyl-1, 10-bathophenanthroline (BPT) system at a drop mercury electrode was investigated in a buffer solution of 0. 02 mol/L HAc-NaAc(pH 4.02). The V(Ⅴ)-BPT complex produces a reduction peak at - 0.36 V(vs. SCE). In the presence of 1.2 ×10-3 % polyvinyl alcohol (PVA), the detection limit and the linear range of the single-sweep sec- and order derivative osillopolagraphic wave were 9. 0 × 10-9 mol/L and 5.0 × 10-8 - 4 .0×10-6 mol/L V (Ⅴ ), respectively. This method has been applied to the determination of bee V(Ⅴ) in samples of drinking water and carbon steel with satisfactory results. The effects of the concentration of PVA on Ip and Ep of the V(V )-BPT complex, the composition of V(V)-BPT complex and the mechanism of the electrode process were discussed.
【CateGory Index】: O657.14
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