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《Chinese Journal of Analytical Chemistry》 1999-06
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Analysis of 2D-Nuclear Magnetic Resonance for Ru(2,2'-bipyridine)_2(4,4'-dimethyl-2,2'-bipyridine) (PF_6)_2

Wang Peng , Yuan Yi, Zhang Milin, Zhu Guoyi (Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry,Chinese Academy of Sciences, Changchun 130022) (Deparment of Chemical Engineering, Harbin Engineering University, Harbin 150001)  
The 1H and 13C NMR spectra are reported for Ru(2, 2'-bipyridine)2 (4,4'-dimethyl-2,2'-bipyridine)(PF6)2 that may be used as electrochemiluminescent species. Because of the effect of Ru atom on ligands and complex steric configuration, it is difficult to attribute the spectra of the title molecular. By using 2D 1H-1H COSY and 1H-13C COSY methods, the proton and carbon-13 spectra are assigned completely. This also provides a basis for NMR characterization of the similar new compounds.
【Fund】: 国家“九五”攻关重点项目(批准号96-A23-03-01)资助课题
【CateGory Index】: O657.2
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