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Determination of Trace Lead by Anodic Stripping Voltammetry Using Acid Chrome Blue K Modified Solid Paraffin Wax Carbon Paste Electrode

Zhang Haili; Ye Yongkang; Xu Bin (Department of Chemistry,Normal University,Hangshi 435002)  
The solid Paraffin wax carben paste electrode was medified by the acid chrome blue K (ACBK). In 0. 2 mol/L NH3·HO2-NH4Cl solution (pH = 8. 5), lead ion was acctimulated to form PbACBK complex on the chemically modified electrode at the applied potential of - 1.0 V. A sensitive oxidation peak of Pb2+ was observed with anodic tripping voltammetry. The peak potential is 0.11 V (vs. SCE). The 1st differential current-logarithm of concentration relationship is linear from 1.0×10-11 to 1 .0 ×10-5 mol/L. The detection limit is 5 .0×10-12 mol/L.
【CateGory Index】: O657.1
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