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《Chinese Journal of Analytical Chemistry》 2003-04
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Determination of Aloe-emodin, Rhein, Emodin and Chrysophanol in Radix Rhei by Reversed Phase High Performance Liquid Chromatography

Zhang Dan  (School of Pharmacy, Sichuan University, Chengdu 610041) Jiang Xinhui (Department of Pharmacy, Chongqing University of Medical Sciences, Chongqing 400016)  
The aloe-emodin, rhein, emodin and chrysophanol in radix rhei were simultaneously determined by reversed phase-high performance liquid chromatography (RP-HPLC) on a hypersil C 18 column (10 μm, 250 mm×4.6 mm i.d.), using methol-Acetonitrile-water (30∶50∶20 adjusted to pH=2.8 with phosphoric acid), a flow rate of 1.0 mL/min, the detective wavelength was 225 nm. These 4 components were separated completely within 20 minutes under this chromatographic condition. The average recoveries were from 98.8% to 103.3%, its relative standard deviations were from 0.7% to 1.6%. The method is simple and quick with high accuracy, and it is suitable for the assay of the Aloe-emodin, rhein, emodin and chrysophanol for radix rhei and compound preparations of Radix Rhei.
【CateGory Index】: O657.7
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