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《Chinese Journal of Analytical Chemistry》 2004-02
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Sequential Determination of As, Sb, Bi and Sn in Zinc Concentrates by Hydride Generation-Atomic Fluorescence Spectrometry in The Presence of L-Cysteine

Li Yan (Liaoning Entry-Exit Inspection and Quarantine Bureau, Dalian 116001)  
The method for sequential determination of As, Sb, Bi and Sn in zinc concentrates by hydride generation-atomic fluorescence spectrometry (HG-AFS) was studied in the presence of L-cysteine. The recoveries are in the range of 92.8%~105.0% for As, 96.0%~109.3% for Sb, 96.0%~111.6% for Bi and 96 7%~103.7% for Sn by melted down sample at a time. The detection limits are 0.35 μg/L, 0.31 μg/L, 0 19 μg/L and 0.35 μg/L respectively. The method has been applied to the determination of As, Sb, Bi and Sn in zinc concentrations with satisfactory results.
【Fund】: 国家质检总局科研课题 (No .K0 12 1999)
【CateGory Index】: O657.31
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