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《Chinese Journal of Analytical Chemistry》 2004-03
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Microwave-Assisted Extraction of Flavonoids from Acanthopanax Senticosus Harms

Liu Zhongying 1,2, Yan Guoquan1, Bu Fengquan2, Sun Jing1, Li Minjing1, Ding Lan1, Zhang Hanqi *1 (College of Chemistry, Jilin University, Changchun 130021) (Institute of Fronter of Medical Science, Jilin University, Changchun 130023)  
Flavonoids from Acanthopanax Senticosus Harms were extracted by means of a microwave-assisted extraction (MAE) technique. The influence of some operation conditions, such as ethanol content, microwave irradiation time, processing pressure and the ratio of sample weight to solvent volume, on the extraction yield of those compounds has been studied by using orthogonal test and optimization based on multivariate statistics. The experimental results show that the highest extraction yield can be obtained when extraction solvent is 50% ethanl, processing pressure is 700 kPa, microwave irradiation time is 10 minutes and the ratio of sample weight to solvent volume is 1∶[KG-3/5]20. Under the optimum conditions of MAE, there is a 40% increase of the extraction yield of flavonoids as compared with Soxhelt extraction.
【Fund】: 吉林省科技发展计划项目 (No .2 0 0 3 0 5 5 1 7)资助
【CateGory Index】: TQ461
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