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《Chinese Journal of Analytical Chemistry》 2004-04
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The Chromatographic Behavior of Hydroxyanthroquinones from Rheum Palmatum L. on p-tert-Butyl-calix[8]arene-bonded Silica Gel Stationary Phase by High Performance Liquid Chromatography

Li Laisheng 1,2 , Liu Min 1, Da Shilu *1 , Feng Yuqi 1 1(Department of Chemistry, Wuhan University, Wuhan 430072) 2(Analytical and Testing Center, Nanchang University, Nanchang 330047)  
The chromatographic behavior of five hydroxyanthroquinones, including aloe emodin, emodin, physcion, chrysophanol and rhein from Rheum palmatum L. on a new calix[8]arene bonded silica gel stationary phase (CABS) were studied by high performance liquid chromatography (HPLC). The results show that various interactions occur between the analytes and the calix[8]arene bonded phase besides hydrophobic interaction, which are different from that on octadecyl silica (ODS). The inclusion interaction improves the selectivity of CABS to these compounds.
【Fund】: 国家自然科学基金 (No .2 0 2 75 0 2 9);; 教育部优秀青年教师资助计划项目
【CateGory Index】: O657.7
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Chinese Journal Full-text Database 1 Hits
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1 Zhang Dan  (School of Pharmacy, Sichuan University, Chengdu 610041) Jiang Xinhui (Department of Pharmacy, Chongqing University of Medical Sciences, Chongqing 400016);Determination of Aloe-emodin, Rhein, Emodin and Chrysophanol in Radix Rhei by Reversed Phase High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2003-04
2 Zhou Jihong;Yuan Yisheng and Yang Junwei(Nanjing General Hospital of Nanjing Command ,210002);HPTLC Determination of Three Anthraquinone Derivatives of Chinese Rhubarb in Prasma[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;1995-06
3 SHANG Xiao yu, YUAN Zhuo bin (Graduate School, Chines Academy of Sciences, Beijing 100039, China);Isolation of active constituents in rhubarb by micellar electrokinetic capillary chromatography[J];Chinese Traditional and Herbal Drugs;2001-08
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1 Xiao Yuxiu (College of Life Science, Wuhan University, Wuhan 430072) Yue Weihua Da Shilu (College of Chemistry and Environment Science, Wuhan University, Wuhan 430072);HPLC Study of Small Peptides on the Silica-bonded Stationary Phase of Nitrogen containing crown ether[J];AMINO ACIDS & BIOTIC RESOURCES;2000-02
2 LI Jian-xin, ZHANG Xu-mei, XU Qi-shou(Institute of Radiation Medicine,Academy of Military MedicalSciences,Beijing 100850, China);Physiological and Biochemical Effects of Tryptophan and Its Application[J];Amino Acids & Biotic Resources;2005-03
3 Xia Yuzheng Jiao Shuke (Department of Applied Chemistry);Synthesis and Characterization of Glycoturil[J];;1990-03
4 LUO Ai-qin,LIU Li-wen,DAI Rong-ji,ZHANG Jin-zhuan,FANG Min(School of Life Science and Technology, Beijing Institute of Technology, Beijing100081, China);Preparation and Characterization of 4,4-Dihydroxydiphenyl-Joined β-Cyclodextrin Bonded Silica Stationary Phase for High Performance Liquid Chromatography[J];Journal of Beijing Institute of Technology;2004-07
5 LUO Ai-qin~1,LIU Li-wen~(1,2),DAI Rong-ji~1,HAO Jian-wei~1,ZHANG Jin-zhuan~2,FANG Min~2 (1.School of Life Science and Technology, Beijing Institute of Technology, Beijing 100081, China; 2.Fire Command Department, Chinese People's Armed Police Force Academy, Langfang, Hebei 065000, China);Preparation and Chromatographic Performances of 2,6-di-O- Benzyl-β-Cyclodextrin Bonded Silica Stationary Phase[J];Journal of Beijing Institute of Technology;2005-01
6 LUO Ai-qin~1, HOU Ai-jun~1, DAI Rong-ji~1, HAO Jian-wei~1, LIU Li-wen~2(1.School of Life Science and Technology, Beijing Institute of Technology, Beijing100081, China; 2.Chinese People's Armed Police Force Academy, Langfang, Hebei065000, China);Preparation and Investigation of the Chromatographic Performance of Heptakis(2,6-di-O-Butyl)-β-Cyclodextrin Bonded Silica Stationary Phase for High Performance Liquid Chromatography[J];Journal of Beijing Institute of Technology;2005-08
7 LUO Ai-qin1,QIAN Wei1,WANG Fu-ming1,2,LI Yan1,SUN Liquan1,GENG Li-na1(1.School of Life Science and Technology,Beijing Institute of Technology,Beijing 100081,China;2.Department of Chemistry,Dezhou University,Dezhou,Shandong 253023,China);Optimized Conditions of 1-Phenylpropanol Separation on the New Chiral Stationary Phase of Peptide Bonding β-Cyclodextrin[J];Transactions of Beijing Institute of Technology;2007-07
8 SUN Li-quan,DING Guang-hui,MA Ning,GENG Li-na,LUO Ai-qin(School of Life Science and Technology,Beijing Institute of Technology,Beijing 100081,China);Preparation and Application of the Chiral Stationary Phase of New CBZ-Phenylalanine-β-Cyclodextrin Bonded Silica for High Performance Liquid Chromatography[J];Transactions of Beijing Institute of Technology;2008-08
9 SU Xue-li 1,WU Cai-ying 2 (1.Chem.Research Inst., Jingmen Vocational Technical College Jingmen 448000,Hubei,China; 2.Chem. School, Wuhan Univ,Wuhan 430072, Hubei,China);The separation of Grob mixtures by calixarene as chromatography phases stationary[J];Journal of Baoji College of Arts and Science(Natural Science Edition);2002-04
10 Wang Xu;Studying the Way of How to Investigate the Active Principles of Usually Used Chinese Traditional Drugs[J];;1982-04
【Secondary Citations】
Chinese Journal Full-text Database 3 Hits
1 Cao Hong and Liu Yun(Institute for Drug Control of PLA,Beijing,100071);Determination of Rhein,Emodin,Chrysophanol,Physcion and Aloe-emodin in JinYiNiaoShi Granules and Radix Rhei by HPLC[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;1998-01
2 YY Zong,MT Yu,ZQ Zhu and CT Che (Qinghai Institute of Druy Control, Xining 810000; Guangzhou Bai Yun Shan Pharmaceutical Factory,Guangzhou 510515; Depatrtment of Chemistry, Hong University of Science and Technology);MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY SEPARATION AND DETERMINATION OF CHINESE TRADITIONAL MEDICINE──SEVERAL RHEUM SPECIES[J];ACTA PHARMACEUTICA SINICA;1995-08
3 ChengXin;Cheng Yuying;Hu YuZhu;Yang Qinghua (Department of Analytical Chemistry,China Pharmaceutical University,Nanjing 210009);Determination of Emodin in Niuhuang Jiedu Pian by HPLC and Studies on Method Ruggeddness[J];JOURNAL OF CHINA PHARMACEUTICAL UNIVERSITY;1994-06
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