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《Chinese Journal of Analytical Chemistry》 2004-10
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Structural Elucidation on a Triterpenic Heptaglycoside from Kalopanax Septemlobus

Yin Jianyuan, Yang Xiaohong, Meng Qin,Wang Ensi* (College of Pharmacy,Jilin University,Changchun 130021)  
The ethanolic extract of the bark of Kalopanax septemlobus (Thunb.) Koidz. isolated a triterpenic heptaglycoside(1), the structure of which was characterized by chemical and spectral means (infrared (IR),electrospray ionization-mass spectrometry (ESI-MS), 1H nuclearomagnetic resonance (NMR), 13C NMR, 1H-1H correlatim spectroscopy (COSY), 1H-1H total correlation spectroscopy (TOCSY),heteronuclear multiple quantum correlation (HMQC),heteronuclear multiple bond correlation (HMBC)) as 3-O-β-D-xylopyranosyl-(1→4)- β-D-xylopyranosyl -(1→3)-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranosyl hederagenin 28-O-α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→6)-β-D-glucopyranoside,namely septemloside Ⅰ.
【CateGory Index】: O629
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