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《Chinese Journal of Analytical Chemistry》 2004-12
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Determination of 7,8-Dihydroxyl-coumarin in Roots,Stems, Leaves and Flowers of Stellera Chamaejasme L. by High Performance Liquid Chromatography

Tian Shangyi, Wei Chunyan*, Zhou Daowei, Feng Na, Pan Rui(Institute of Grassland Science, Northeast Normal University, Key Laboratory for Vegetation Ecology,Ministry of Education, Changchun 130024)  
A determination method of 7,8-dihydroxy-coumarin in roots, stems, leaves and flowers of Stellera chamaejasme L. by reversed-phase high performance liquid chromatography was established and at the same time the purity of 7,8-dihydroxy-coumarin was detected by means of Diode-Array Detector. The chromatographic column, Alltech C_~18 (250 mm×4.6 mm, 5 μm), methanol-water(40∶60,V/V) mobile phase with ~1.0 mL/min flow rate, the detected wavelength (326 nm), and the column temperature (28℃) were ~adopted . The calibration curve was linear under the concentration of 1.4~880 mg/L, the correlation coefficient was ~over 0.9999, the detected limit was 0.2 mg/L(3σ). The contents of 7,8-dihydroxy-coumarin in roots, stems, leaves and flowers of Stellera chamaejasme L. were 0.37%, 0.58%, 1.76% and 1.60%, ~respectively . The ~recovery was 95.8%~100.8% and RSD was 1.9% (n=6). The method is simple, accurate and has wider linear range. The method can be adapted to evaluate the quality of medicinal plants that contain ~7,8-dihydroxy -coumarin.
【Fund】: 国家重点基础研究发展规划项目(NO.G2000018606)
【CateGory Index】: O657.7
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