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《Chinese Journal of Analytical Chemistry》 2005-09
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Determination of Trace Germanium in Ganoderma by Hydride Generation-Atomic Fluorescence Spectrometry

Song Xuejie~1,2, Zhang Feng~1, Duan Taicheng~1, Guo Pengran~1,2, Chen Hangting~1 ~1(State Key Laboratory of Electroanalytical Chemistry, National Analytical Research Center of Electrochemistry & Spectroscopy, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022) ~2(Graduated School of Chinese Academy of Sciences, Beijing 100039)  
A method for the determination of total Ge in ganoderma samples by hydride generation-atomic fluorescence spectrometry (HG-AFS) was developed. By using microwave assisted digestion procedure, organic Ge could be destroyed successfully and element loss caused by the chlorine existing in samples could be avoided. Working conditions of AFS-920, optimum conditions for the generation of volatile of Ge species and microwave assisted procedure were optimized. Optimum acidity of the sample solution was 20% H_3PO_4 and the signal intensity was increased with the presence of 5% H_2SO_4. Comparison was made between the results obtained by two sample digestion procedures: microwave assisted procedure and dry ashing treatment. The detection limit and RSD of this method were 0.83 μg/L and 1.26%, respectively. The recoveries ranged from 84.0% to 96.5%.
【Fund】: 科技部新技术、新方法专项资助(No.科2004-51)
【CateGory Index】: O657.31
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Chinese Journal Full-text Database 7 Hits
1 CHEN Qi-hang et al(College of Food Science,Henan Agricultural University,Zhengzhou,Henan 450002);Study on Analytical Methods of Trace Element Germanium in Agricultural Products[J];Journal of Anhui Agricultural Sciences;2007-14
2 XU Zhen-Rong1,MA Xiao-Ling2,JIA Xiao-Yu3,4,HAN Yi3,4,DUAN Tai-Cheng3,CHEN Hang-Ting3 1(Shanghai Food Production Administration,Shanghai 201800)2(Preekem Scientific Instruments Co.Ltd.,Shanghai 201108)3(Graduate School of Chinese Academy of Sciences,Beijing 100039)4(State Key Laboratory of Electroanalytical Chemistry,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022);Determination of Inorganic Germanium in Health Foods by Inductively Coupled Plasma Optical Emission Spectrometry with Chloride Generation[J];Chinese Journal of Analytical Chemistry;2011-04
3 LI Gong-hai,SHEN Chong-yu,JIANG Yuan,CHEN Xiao-wei,CHEN Hui-lan,WU Bin and ZHAO Zeng-yun(Jiangsu Entry-Exit Inspection and Quarantine Bureau,Nanjing 210001);Determination of trace germanium and selenium in health food by hydride generation-atomic fluorescence spectrometry[J];Chinese Journal of Analysis Laboratory;2007-03
4 SHU Yong-hong1,2 and He Hua-kun*1(1.Chinese National Analytical Center,Guangzhou 510070,2 Guangdong Key Laboratory of Chemical Emergency Test),Fenxi Shiyanshi,2007,26(8): 106~122;Atomic absorption spectrometry and atomic fluorescence spectrometry[J];Chinese Journal of Analysis Laboratory;2007-08
5 LIAN Xi-jun, LU Xiao-xiang, LIU Qin-sheng, ZHAO Guang-li, XI Jun (College of Biotechnology and Food Science, Tianjin University of Commerce,Tianjin 300134,China);THE STUDY ON DETERMINATION OF β-GLUCAN BY FLUORIMETRY WITH SODIUM FLUORESCEIN[J];Food Research and Development;2006-10
6 WANG Chang1,GUO Peng-ran1,2,CHEN Hang-ting3,OU Hong1 (1.Guangdong Key Laboratory of Chemical Emergency Test,China National Analytical Center(Guangzhou),Guangzhou 510070,China;2.School of Environmental Science and Engineering,Sun Yat-sen University,Guangzhou 510275,China;3.National Analytical Research Center of Electrochemistry and Spectroscopy,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China);Application of Hydride Generation Atomic Fluorescence Spectrometry on Analysis of Trace Metal Elements in Chinese Traditional Medicine[J];Journal of Instrumental Analysis;2009-04
7 DUAN Min1 and LI Guili2(1.College of Life Science Northwest A&F University,Yangling Shaanxi 712100,China;2.College of Economics and Management,Northwest A&F University,Yangling Shaanxi 712100,China);The Determination of Trace Ge in Fresh Grape by HG-AFS[J];Acta Agriculturae Boreali-Occidentalis Sinica;2009-02
Chinese Journal Full-text Database 3 Hits
1 LIU Xian Guo (Hankou Branch,China University of Geosciences,No.15 Hangkonglu,Hankou,Wuhan 430030,P.R.China) FANG Jin Dong (Geological Experiment Institute of Hubei,Wuhan 430022,P.R.China);Determination of Trace Germanium in Geochemical Samples by Hydride Generation-Atomic Fluorescence Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2002-01
2 CHEN QingchuanResearch Center for EcoEnvironmental Sciences,Academia Sinica,100085 BeijingYANG HuifenInstitute for Food Safety Control and Inspection,Ministry of Public Health,100021 Beijing;RESPECTIVE DETERMINATION OF INORGANIC GERMANIUM AND GERMANIUM132 IN FOODS[J];SPECTROSCOPY AND SPECTRAL ANALYSIS;1998-01
Chinese Journal Full-text Database 10 Hits
1 ZHANG Wan-feng(Shaanxi Normal University,Xi′an,Shaanxi 710061);Rapid Determination of Se in Se-enriched Tea in Ziyang area of Ankang City by Using Flame Atomic Absorption Spectrometry[J];Journal of Anhui Agricultural Sciences;2008-15
2 WANG Duo et al(Horticulture Department of Shanxi Agricultural University,Taigu,Shanxi 030801);Effects and Action Mechanisms of Organic Germanium on Plant[J];Journal of Anhui Agricultural Sciences;2009-11
3 XIANG Jiming 1, FANG Wenxin 2, JIN Zhaoyang 1, CEI Jiangchen 1 (1.The Chemistry & Life-science Department, Ankang Teachers College; 2.The Health Department of Hanbin District, Ankang 725000, China);Determination of Trace Selenium in Tea of Qinba by Flame Atomic Absorption Spectrometry[J];Journal of Ankang Teachers College;2002-04
4 SUN Han wen (Department Chemistry of Hebei University,Baoding 071002), SUO Ran (Department of Food Science,Hebei Agricultural University,Baoding 071001), LU Yun kai and ZHANG De qiang (Department Chemistry of Hebei University,Baoding 071002),F;Determination of Trace Germanium in Edible Fungus by Atomic Fluorescence Spectrometry Using Hydride Generation with Alkaline Mode[J];Analytical Laboratory;2001-01
5 QIU Hai-ou, ZHENG Hong-tao and TANG Zhi-yong (Faculty of Material science and Chemical engineering,China University of Geosciences, Wuhan,430074);Development in Analysis Technique of Atomic Absorption and Atomic Fluorescence Spectrometry[J];Analytical Laboratory;2003-01
6 CHEN Wen-bin, XU Xing-you, MA Wei-xing and LI Yan-hui(Department of Chemical Engineering. Huaihai Institute of Technology, Lianyungang 222005);Determination of trace amount of germanium by spectrophotometry with T(DBNP)P[J];Analytical Laboratory;2005-09
7 LIU Yan-juan, ZHANG Chong-yu(College of Agriculture, Guizhou University, Guiyang, Guizhou 550025, China);Study on the Determination Method of Germanium in Soil by Atomic Fluorescence Spectrometry[J];Guizhou Agricultural Sciences;2009-02
8 TANG Jia-Hua LI Lei CHANG Shi-Ke CHEN Tian-Yun (Department of Chemistry,Chaohu College,Chaohu,Anhui 238000,P.R.China);Spectrophotometric Method on Germanium-2-Hydroxy-3-Methoxyphenylfluorone-CTMAB System[J];Chinese Journal of Spectroscopy Laboratory;2004-06
9 TIE Mei 1,2, ZHANG Wei2 , LI Jing2, JING Kui2, ZANG Shu-liang 2*, LI Hua-wei31. Department of Chemistry, East China Normal University, Shanghai 200062, China2. Environmental Science Department of Liaoning University, Shenyang 110036, China3. College of Environmental and Life Sciences, Shenyang Normal University, Shenyang 110034, China;Determination of Trace Selenium in Edible Fungi with Graphite Furnace Atomic Absorption Spectroscopy[J];Spectroscopy and Spectral Analysis;2006-01
10 JIN Wei, ZHAO Cheng-yi, MA Hui Analytical and Testing Center, Beijing Normal University, Beijing 100875, China;Determination of Trace Germanium by HG-ICP and Study on the Medium Influence[J];Spectroscopy and Spectral Analysis;2006-09
Chinese Journal Full-text Database 10 Hits
1 ZHOU Min~1 (1.Changsha Environment Protection Technical College,Changsha 410004,China);The Lead and Cadmium Content of the Soil and Vegetables Extraction and Flame Ion Absorption Method[J];Environmental Science and Management;2006-03
2 LIANG Yun-zhang , DING Chang-jiang (Laboratory of Ion Beam Bioengineering, Inner Mongolia University, Hohhot, Nei Monggol 010021, China; College of Science, Inner Mongolia Polytechnic University, Hohhot, Inner Monggol 010062, China);EHD Analysis of the High Voltage Electric Field Drying Technology's Principle[J];Journal of Beijing Institute of Technology;2005-S1
3 XIE Hualin,WEN Haichu(Department of Chemical Engineering,Hunan Building Materials College,Hengyang 421008,China);Study on the Determination of Trace Amount of Antimony in Enamel Vessel by Hydride Generation-Atomic Fluorescence Spectrometry[J];Glass & Enamel;2005-01
4 WANG Jia-sheng(Fujian Anxi Minhua Storage Battery Co., Ltd.,Anxi,Fujian 362400,China);Determination of arsenic in lead ingots with a flow injection quartz tube atomic absorption spectrometry[J];Chinese Labat Man;2005-01
5 WANG Li , WANG Jin-ying (Tianjin Environmental Monitoring Center,Tianjin300191,China);Determination of Lead in Gasoline by Flame Atomic Absorption Spectrophotometer with Isopropanol as Solvent[J];Urban Environment & Urban Ecology;2005-01
6 ZHU Wen-yuan~1,DENG Zhi-cheng~2(1.Department of Biochemist, Guangzhou Medical College,Guangzhou510182,China;2.College of Light Industry and Chemical Engineering,Guangdong University of Technology,Guangzhou510090,China);Determination of mercury content in freckle cream by atomic fluorescence spectrometry[J];China Surfactant Detergent & Cosmetics;2004-06
7 Mao Yunfei Jiang Yechao (Yangzhou Chemical Engineering School,Yangzhou 225007);To Determine Ge by Spctrophotometric of DBHPF[J];Journal of Chongqing Polytechnic College;2000-04
8 Jiang Li (Environment Monitoring Station,Chongqing Gas Mine,Southwest Oil & Gas Field,Chongqing 400021);Determination of Trace Amounts of Arsenic in Gas Field Sewage by Hydride Generation-Atomic Fluorescence Spectrometry[J];Chongqing Environmental Science;2001-01
9 JING Li-xin~1,CAO Li-li~1,QIU Hong-jiu ~1,YANG Li-jun~2,LIU Min ~2,ZHANG LI-min~2 (1. Medical College, Dalian University ,Dalian 116622, China; 2.Dalian Sanitation and Antiepidemic Station,Dalian 116021, China );Determination of trance elements in new preparation -component F3 of astragalus membranaceus by ICP-AES[J];Journal of Dalian University;2004-02
10 LIAN Xi-jun LU Xiao-xiang LIN Xu-hui WANG Feng-ling (Biotechnology and Food Science Institute, Tianjin University of Commerce, Tianjin 300134,China);Mixed Linkage Beta - glucan Assay Procedure in Barley Seeds and Goods[J];;2005-04
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 XU Zhen-Rong1,MA Xiao-Ling2,JIA Xiao-Yu3,4,HAN Yi3,4,DUAN Tai-Cheng3,CHEN Hang-Ting3 1(Shanghai Food Production Administration,Shanghai 201800)2(Preekem Scientific Instruments Co.Ltd.,Shanghai 201108)3(Graduate School of Chinese Academy of Sciences,Beijing 100039)4(State Key Laboratory of Electroanalytical Chemistry,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022);Determination of Inorganic Germanium in Health Foods by Inductively Coupled Plasma Optical Emission Spectrometry with Chloride Generation[J];Chinese Journal of Analytical Chemistry;2011-04
2 TANG Zhi-yong,QIU Hai-ou and ZHENG Hong-tao(Faculty of Materia Science and Chemical engineering,Chin University of Geosciences,Wuhan 430074);Analysis of rocks and minerals[J];Chinese Journal of Analysis Laboratory;2008-10
3 RUAN Xina,b LI Xiu-Yongb WANG Xiao-Jiec YANG Li-Hongc a(College of Food Science and Engineering of Ocean University of China,Qingdao,Shandong 266003,P.R.China)b(Yantai Entry-Exit Inspection and Quarantine Bureau,Yantai,Shandong 264000,P.R.China)c(Ludong University,Yantai,Shandong 264000,P.R.China);Determination of Selenium in Peas by Hydride Generation-Atomic Fluorescence Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2007-06
4 ZHAO Danqing,SUN Zhancai,ZHANG Li (College of Chemistry and Chemical Engineering,Inner Mongolia University for Nationalities, Inner Mongolia Tongliao 028042,China);Determination of Germanium in Mongolia Medicine Naru Sanwei Pill by Polarography[J];Guangdong Trace Elements Science;2011-02
5 BAI Zhong-chen,QIN Shui-jie(Laboratory for Photoelectric Technology and Application,Guizhou University,Guiyang 550025,China);Study on fluorescent detection for glucose molecule in microchannels[J];Journal of Sichuan University(Natural Science Edition);2007-05
6 GONG Qiao-juan,YANG Hai-ying(Department of Application Chemistry,Yuncheng University,Yuncheng 044000,China);Determination of Selenium in Black Peanut by Graphite Furnace Atomic Absorption Spectrometry[J];Journal of Instrumental Analysis;2011-02
7 ZHAO Chun-yan1,2,ZENG Ya-wen2,3*,PU Xiao-ying2,YANG Shu-ming2,DU Juan2(1.Faculty of Agronomy and Biotechnology,Yunnan Agricultural University,Yunnan Kunming 650201,China;2.Biotechnology and Genetic Resources Institute,Yunnan Academy of Agricultural Sciences,Yunnan Kunming 650205,China;3.Agricultural Biotechnology Laboratory of Yunnan,Yunnan Kunming 650223,China);Determination of Functional Compositions in Different Barley Cultivars(lines) by Spectrophotometry[J];Southwest China Journal of Agricultural Sciences;2010-03
8 ZHENG Da-zhong,ZHENG Ruo-feng,WANG Hui-ping(Chengdu Testing Center of Integrated Rock Mine,Chengdu,610081,China);Application of Nanometer Materials in Environment Protection and Testing Field[J];Journal of Salt Lake Research;2008-04
9 LI Dan,LI Biao(Hubei Geology Experiment Research Institute,Wuhan 430034,China);Progress on the analysis of trace germanium[J];Metallurgical Analysis;2010-12
10 WU Qing-hui1, HUANG Bo-xi2, YANG Yun-yun1, ZHANG Zhi-jun1, HUANG Xuan-ying1 (1. Guangdong Provincial Public Laboratory of Analysis and Testing Technology,China National Analytical Center,Guangzhou 510070,China; 2. Guangdong Inspection and Quarantine Technology Center,Guangzhou 510623,China);Determination on the content of total arsenic in the Liushen Pills and its content of soluble arsenic in artificial intestinal juice by AFS[J];Chinese Traditional Patent Medicine;2010-08
China Proceedings of conference Full-text Database 1 Hits
【Secondary Citations】
Chinese Journal Full-text Database 2 Hits
1 Chen Qingchuan; Yang Huifen(Institute of Food Safety Control and Inspection, The Ministry of Public Health. No.7 Panjiayuan, Chaoyang District. Beijing 100021, P.R.China);Progress in the Photometric Analysis of Germanium[J];CHINESE JOURNAL OF SPECTROSCOPY LABORATORY;1994-06
2 Guo Xiao-wei;Determination of Trace Amount of Selenium and Tellurium in Geological Samples by Hydride Generation Nondispersive Atomic Fluorescence Spectrometry[J];;1983-04
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