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《Chinese Journal of Analytical Chemistry》 2006-05
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Influence of Near Infrared Spectral Resolution on the Quantitative Analysis

Wang Yibing1, Wang Hongyu2,Zhai Hongju1, Lu Fei1, Wu Weihong1,Wang Haishui*1, Xi Shiquan11(Laboratory of Rare Earth Chemistry and Physics, Changchun Institute of Applied Chemistry,Chinese Academy of Sciences, Changchun130022)2(Jilin University, Changchun130022)  
Near infrared (NIR) spectra of 50 powder samples containing acetaminophen and ethenzamidewere measured with spectral resolution 1, 4 and 8 cm-1respectively, and the calibrations were made fromthese NIR spectra for the properties of acetaminophen and ethenzamide. The best calibration for acetamino-phen, which provides a SEE (the standard deviation from the property residuum) about0.20 both for calibra-tion set and validation set spectra, was built with 4 cm-1spectral resolutions. Both higher resolution(1 cm-1) and lower resolution ( 8 cm-1) spectra provide a little worse calibration results. The above calibra-tion results demonstrate that the spectral resolution has an important effect on the calibration results and thesuccessful application of NIR is highly dependent on the proper selection of spectral resolution.
【Fund】: 国家自然科学基金(No.90306001、20273068)资助项目
【CateGory Index】: O657.33
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