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《Chinese Journal of Analytical Chemistry》 2006-06
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Rapid Analysis of Multiresidual Pesticides in Agricultural Products by Gas Chromatography-Mass Spectrometry

Liu Libin~1,Hashi Yuki~2,Qin Yaping~2,Zhou Haixia~2,Lin Jinming~(*1)()~1(State Key Laboratory of Environmental Chemistry and Ecotoxicology,Research Center forEco-Environmental Sciences,Chinese Academy of Sciences,Beijing 100085)()~2(Shimadzu(HongKong) Limited,Beijing Office,Analytical Applications Center 14F No.16,Chao Yang Men Wai Street,Life Tower Chao Yang District,Beijing 100020)  
A method for rapid analysis of multiresidual pesticides in agricultural products by gas chromatograph-mass spectrometry(GC/MS) was introduced.Matrix solid-phase dispersion(MSPD) technique with slight modification was employed to minimizing matrix interferences.To evaluate the performance of the(system),97 target pesticides were spiked into a range of food including potato,cabbage,carrot,apple,(orange),cucumber and rice.The combination of MSPD technique and GC/MS for analysis of 97 pesticides can be accomplished within 90 min per sample.Most pesticides were recovered in the range of 70%-120% with relative standard deviation(RSD) 10%.The results demonstrated that the method could be successfully applied to a broad range of target pesticides in a diverse range of food materials.
【Fund】: 国家自然科学基金重点项目(No.20437020);; 中国科学院重要方向性项目(No.KZCX3-SW-432)
【CateGory Index】: TS207.53
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