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《Chinese Journal of Analytical Chemistry》 2008-01
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Structural Identification of Phenylpropanoids from Vernonia Chunii

Yuan Ke1,Jia An2,Zhu Jian-Xin21(College of Food and Pharmacy,Zhejiang Forestry University,Lin'an 311300)2(College of Pharmacy,Henan University of Traditional Chinese Medicine,Zhengzhou 450008)  
To study the chemical constituents of Vernonia chunii of Hainan province,the constituents were separated and purified by column chromatography with macroporous adsorption resin Diaion HP-20,Sephadex LH-20,Toyopearl HW-40(C),MCI Gel CHP-20,RP-18 and normal phase silica gel.Their structures were identified on the basis of physiochemical properties and spectral methods(1H NMR、13C NMR、distorsionless enhamecment by polarization transfer(DEPT),1H-1H correlation speclroscopy(1H-1H COSY),helernuclear single quantum correlation(HSQC),heternuclear multiple bond correlation(HMBC),ESI-MS,IR).Seven compounds were isolated and identified as:3,2'-bis(3,4-dihydroxyphenyl)-5,3'-dihydroxy-6,7-combine dihydropyran-3,4-dihydro-benzopyrone(Ⅰ),1,3-di-o-caffeoylquinicacid(Ⅱ),1,5-di-o-caffeoylquinicacid(Ⅲ),1-(3,4-dimethoxyphenyl)-2,3-dimethanol-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene(Ⅳ),Chlorogenic acid(Ⅴ),Caffeic acid(Ⅵ)and Ferulic acid(Ⅶ).CompoundⅠis a new compound,the other componuds were isolated from this plant for the first time.
【CateGory Index】: R284
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