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《Chinese Journal of Analytical Chemistry》 2009-03
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Synthesis and Properties Study of Mercury Ion Imprinted Polymer

WANG Zhu-Qing,SHEN Yu-Yong,WU Gen-Hua,HE Chi-Yang(College of Chemistry and Chemical Engineering,Anqing Normal College,Anhui Key Laboratory of Functional Coordination Compounds,Anqing 246011)  
A new type of Hg2+ imprinted polymer was prepared by a double-imprinting approach for the selective separation of Hg2+ from aqueous solution.In the imprinting process,both mercury ions and surfactant micelles(cetyltrimethylammonium bromide) were used as templates,N-[3-(trimethoxy-silyl)propyl]ethylenediamine as functional monomer,and tetraethoxysilane as cross-linking agent.The mercury ions and surfactant were removed from polymer via acid leaching and ethanol extraction,respectively.The adsorption property and selective recognition ability of the polymer were studied by equilibrium-adsorption method.Results showed that in the presence of Cu2+ or Cd2+,the largest relative selectivity coefficient(k') of the ion-imprinted polymer was over 200,and the polymer could be used repeatedly.
【CateGory Index】: O631.3
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