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《Chinese Journal of Analytical Chemistry》 2009-11
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Simultaneous Determination of Catechol and Hydroquinone at Electrospun Palladium Nanoparticle/Carbon Nanofibers Modified Electrode

ZHANG Hai-Jiang1,WANG Chun-Yan2,HUANG Jian-She1,YOU Tian-Yan 1 1 ( State Key Laboratory of Electroanalytical Chemistry,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022) 2 ( Institute of Food Engineering,Jilin Teacher's Institute of Engineering and Technology,Changchun 130052)  
Palladium nanoparticle/carbon nanofibers( Pd/CNFs) were prepared by electrospinning technique with subsequent thermal treatments and were employed to modify glassy carbon electrode ( Pd/CNF-GCE / CME). Pd/CNF-GCE /CME exhibited excellent electrocatalytic activities towards catechol and hydroquinone,and the reversibility of catechol and hydroquinone were significantly improved. The effects of pH value on the oxidation peak current and potential of catechol and hydroquinone were studied by differential pulse voltammetry( DPV) ,and 0. 1 mol/L PBS( pH 8. 0) was selected as the supporting electrolyte. Under the optimized conditions,the oxidation peak current of catechol was linearly with the concentration of catechol in the range of 1 -90 μmol/L in the presence of 50 μmol/L hydroquinone with the detection limit of 0. 3 μmol/L( S/N = 3) and the oxidation peak current of hydroquinone was linearly with the concentration of hydroquinone in the range of 2 -100 μmol/L in the presence of 50 μmol/L catechol with the detection limit of 1. 0 μmol/L. Furthermore,the modified electrode exhibited good reproducibility and selectivity. The modified electrode has been used for the determination of catechol and hydroquinone in imitative water samples with satisfactory results.
【Fund】: 国家自然科学基金(Nos.20605020 20875085)资助项目
【CateGory Index】: O657.1
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【References】
Chinese Journal Full-text Database 10 Hits
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1 ZHOU Xue-chou*,ZHENG Xin-yu,Lü Ri-xin and Wang Yu-Lin(College of life Sciences,Fujian Agriculture and Forestry University,Fuzhou 350002);Study on the voltammetric behaviour and detection of quercetin at a poly(glutamic acid) modified glassy carbon electrode[J];Chinese Journal of Analysis Laboratory;2012-05
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3 HE Chun-Lan1,LIU Cheng-Lun1,XIE Tai-Ping2,WANG Yuan1,ZHANG Jing1,ZHANG Liang1 (1.College of Chemistry & Chemical Engineering,2.State Key Laboratory of Coal Mine Disaster Dynamics and Control,Chongqing University,Chongqing 400044,China);Preparation of Graphene and Electrocatalysis Oxidation of p-Hydroquinone at Graphene Modified Electrode[J];Chemical Journal of Chinese Universities;2012-06
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9 Zhang Yan 1,Wei Shaohong 2,Chen Songtao 1(1.Department of Environmental and Municipal Engineering,Henan University of Urban Construction,Pingdingshan Henan 467036,China;2.College of Chemistry and Chemical Engineering,Anyang Normal University,Anyang Henan 455000,China);Preparation of Polycrystal Violet Film Modified Electrode and Determination of Hydroquinone and Catechol in Water[J];Environmental Protection of Chemical Industry;2013-03
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