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《Chinese Journal of Analytical Chemistry》 2013-02
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Determination of Trace Cadmium and Lead in Water Based on Graphene-modified Platinum Electrode Sensor

TANG Feng-Jie1,2,ZHANG Feng1,2,JIN Qing-Hui1,ZHAO Jian-Long1 1(State Key Lab of Transducer Technology,Shanghai Institute of Microsystem and Information Technology, Chinese Academy of Sciences,Shanghai 200050,China) 2(University of Chinese Academy of Sciences,Beijing 100039,China)  
Graphene,grow on platinum electrode(prepared with the method of micro-electromechanical system) with CVD,was used in combination with in situ plated bismuth film electrode for fabricating the enhanced electrochemical sensing platform to determine trace cadmium(Cd2+) and lead(Pb2+) by differential pulse anodic stripping voltammetry(DPASV).The sensor is three-electronic system that consisted of graphene-modified platinum(G/Pt) working electrode,Ag/AgCl reference electrode and platinum wire auxiliary electrode.The experiment result showed that the sensor performed well in simultaneously detecting Cd2+ and Pb2+.The linear calibration curves ranged from 0.05 mg/L to 10 mg/L for Cd2+ and 0.03 mg/L to 5 mg/L for Pb2+.The detection limits were estimated to be around 10 μg/L for Cd2+and Pb2+.This method is simple,safe,fast and good reproducibility,and can be used for rapid detection of Cd and Pb in wastewater,surface water and domestic water.
【Fund】: 国家973计划(Nos.2012CB933303 2011CB707505);; 国家科技支撑计划(No.2012BAK08B05);; 上海市科委(Nos.11391901900 11530700800 11ZR1443900 10391901600)资助项目
【CateGory Index】: X832;O657.1
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