Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chinese Journal of Analytical Chemistry》 2013-06
Add to Favorite Get Latest Update

Determination of 19 Quinolone Antibiotics in Cosmetics by Ultra Performance Liquid Chromatography

CHEN Jing,ZHENG Rong,JI Shen,WANG Ke(Shanghai Institute of Food and Drug Control,Shanghai 201203,China)  
An ultra-liquid chromatographic(UPLC) method has been developed for the simultaneous determination of 19 quinolone antibiotics in cosmetics,ofloxacin,norfloxacin,ciproxacin,bifloxacin,sarafloxacin,oxolinic acid and flumequin etc.Different forms of cosmetic samples were prepared by ultrasonic extraction.The extraction solutions were obtained by high-speed centrifugation,the supernatant was degreased by hexane,and then was filtered by 0.22 μm millipore filter,and the continued filtrate was taken for analysis.A Waters reversed phase column,ACQUITY UPLC BEH Shield RP C18(100 mm×2.1 mm,1.7μm) was used with methanol : acetonitrile(85 ∶ 15,V/V)-0.05 mol/L phosphate buffer(pH=3.6) as the mobile phase under the condition of gradient elution.And the diode array detector was used for the determination.The relative standard deviations(RSD) were 0.4%-1.1%;recoveries were 75.5%-105.1%;a variety of quinolones showed good linearity within the concentration range of 5-100 mg/L,correlation coefficients were greater than 0.996;detection limits were 1.2-14.7 mg/kg.This method has been successfully used for the determination of quinolone antibiotic in cosmetics products.
【CateGory Index】: TQ658;O657.72
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 5 Hits
1 LIU Peng-Yan*,SHEN Jie,LIU Lei (College of Chemistry and Environmental Sciences,Heibei University,Baoding 071002,China);Determination of Fluoroquinolones in Grass Carp by High Performance Liquid Chromatography-Ion Trap Mass Spectrometry Using Mixed-templates Imprinted Polymer Extraction[J];Chinese Journal of Analytical Chemistry;2012-05
2 SUN Liang-juan*,LI Hong-quan,LIU Yi-feng,WU Zhi-qiang,HONG Wu-xing,HOU Cui-li(Zhanjiang Entry-Exit Inspection and Quarantine Bureau,Zhanjiang 524001,China);Determination of 14 quinolones and sulfonamides medicine residuces in aquatic product using high performance liquid chromatography-electrospray ionization tandemmass spectrometry[J];Chemical Reagents;2012-07
3 GAO Fudie1,2,ZHAO Yan3,SHAO Bing1,2,ZHANG Jing1,2(1.School of Public Health and Family Medicine,Capital Medical University,Beijing 100069,China; 2.Beijing Key Laboratory of Diagnostic and Traceability Technologies for Food Poisoning, Beijing Centers for Diseases Control and Prevention,Beijing 100013,China; 3.Nanjing Institute of Supervision and Testing on Product Quality,Nanjing 210028,China);Determination of residues of pesticides and veterinary drugs in milk by ultra performance liquid chromatography coupled with quadrupole-time of flight mass spectrometry[J];Chinese Journal of Chromatography;2012-06
4 ZHENG Yan-ming,GUO Xin-dong,XIAN Yan-ping,DU Zhi-feng,LUO Hai-ying,WU Yu-luan,LI Hui-yong(Guangzhou Quality Supervision and Testing Institute,Guangzhou 510110,China);Determination of Seven Fluoroquinolones in Cosmetics by Reversed-phase High Performance Liquid Chromatography[J];Journal of Instrumental Analysis;2009-02
5 Li Lili,Luo Yi,He Songhua,Huang Lili(Guangxi Institute for Food and Drug Control,Nanning 530021,China);Simultaneous determination of 8 quinolone residues in fish meat by high performance liquid chromatography-tandem mass spectrometry[J];Chinese Journal of Food Hygiene;2012-01
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 QUAN Ying,ZHAN Yue-hua,ZHANG Gen-hua,GU Xin-qi,WANG Qing-bai (School of Biology and Food Engineering,Changshu Institute of Technology,Changshu 215500,China);Simultaneous Determination of Nine Quinolone Antibiotics Residues in Food Samples by Ultra Performance Liquid Chromatography-electrospray Tandem Mass Spectrometry[J];Journal of Changshu Institute of Technology;2010-02
2 HUANG Wen-jing,HONG Jian-wen,JIANG Zhong-jun,ZHAO Yan-ting(Guangdong Institute for Drug Control,Guangzhou,Guangdong Guangzhau 510180,China);Determination of Ofloxacin and Ciprofloxacin in Cosmetics by HPLC-DAD[J];Guangzhou Chemical Industry;2010-06
3 XU Wan-bang,ZHANG Li,LIU Ya-xiong,JIANG Zhong-jun(Guangdong Institute of Drug Control,Guangdong Guangzhou 510180,China);Determination and Extracted Directly of Fluoroqronolone in Cosmetics by HPLC[J];Guangzhou Chemical Industry;2012-07
4 WU Xiao-Lian1,2,XIANG Lei2,MO Ce-Hui2,LI Yan-Wen1,2,JIANG Yuan-Neng2, YAN Qing-Yun2,Lü Xuan2,HUANG Xian-Pei1,2 1(Institute of Hydrobiology,Jinan University,Guangzhou 510632,China) 2(Key Laboratory of Water/Soil Toxic Pollutants Control and Bioremediation of Guangdong Higher Education Institutions, Department of Environment Engineering,Jinan University,Guangzhou 510632,China);Determination of Quinolones in Vegetables Using Ultra Performance Liquid Chromatography-Electrospray Ionization Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2013-06
5 HUANG Wen-jing1△,JIANG Zhong-jun1,HONG jian-wen1,ZHAO Yan-ting2(Guangdong Institute for Drug Control,Guangzhou,Guangdong 510180,China;2 Guangdong Food And Drug Vocational College,Guangdong 510520,China);Determination of Metronidazole,Ofloxacin and Ciprofloxacin in Cosmetics by HPLC[J];Progress in Modern Biomedicine;2010-12
6 XU Lin,LUO Yi,XU Bing-jie(Key Laboratory of Pollution Processes and Environmental Criteria of Ministry of Education,College of Environmental Science and Engineering,Nankai University,Tianjin 300071,China);Simultaneous Determination for 12 Antibiotics in Sediments of Haihe River by HPLC-MS/MS Method[J];Journal of Instrumental Analysis;2010-01
7 ;Determination of four fluoroquinolones residues in pork by LC-MS/MS using microwave-assisted extraction[J];Meat Industry;2012-09
8 XU Wei-Dong, QIN Feng, LI Xiao-Wen, CHEN Gui-Liang (Shanghai Institute of Food and Drug Control, Shanghai 201203, China);Determination of twenty-two sulfonamide residues in pork by matrix solid phase dispersion-high pressure liquid chromatography-high resolution mass spectrometry[J];Journal of Food Safety & Quality;2013-01
9 LEI Yi,HE Jia-wen,HUANG Yan-ting,HUANG Wen-jing(Guangdong Institute for Food and Drug Control,Guangzhou 510180,China);Simultaneous Determination of 12 Banned and Restricted Substances in Anti-acne Cosmetics by High Performance Liquid Chromatography[J];Journal of Instrumental Analysis;2013-03
10 Han Quan1,2,Wang Mei2,Yang Xiao-hui1 and Yang Na2(1 Department of Chemistry and Chemical Engineering,Xi′an University of Arts and Science,Xi′an 710065;2 School of Chemistry and Materials Science,Shaanxi Normal University,Xi′an 710062);Determination of pefloxacin in tablet, human urine and plasma by resonance rayleigh scattering method[J];Chinese Journal of Antibiotics;2011-05
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 QUAN Ying,ZHAN Yue-hua,ZHANG Gen-hua,GU Xin-qi,WANG Qing-bai (School of Biology and Food Engineering,Changshu Institute of Technology,Changshu 215500,China);Simultaneous Determination of Nine Quinolone Antibiotics Residues in Food Samples by Ultra Performance Liquid Chromatography-electrospray Tandem Mass Spectrometry[J];Journal of Changshu Institute of Technology;2010-02
2 Pang Guofang~, Cao Yanzhong, Zhang Jinjie, Jia Guangqun, Fan Chunlin, Li Xuemin, Liu Yongming, Shi Yuqiu (Qinhuangdao Entry-Exit Inspection and Quarantine Bureau, Qinhuangdao 066002);Simultaneous Determination of 16 Sulfonamides in Poultry Meat by High-Performance Liquid Chromatography- Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2005-09
3 GUO De-Hua1,DENG Xiao-Jun* 1,ZHAO Shan-Zhen1,ZHU Jian1,XIA Chong-Fei2,CHEN Shun-Sheng2,SONG Yue3 1 ( Shanghai Entry-Exit Inspection and Quarantine Bureau,Shanghai 200135) 2 ( Shanghai Fishery University,Shanghai 200433) 3 ( China Pharmaceutical University,Nanjing 211198);Simultaneous Determination of 76 Veterinary Drug Residues in Foodstuffs of Animal Origin by Solid Phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2010-03
4 HE Qiang1,KONG Xiang-hong1,LI Jian-hua1,YUE Ai-shan1 and MA Yu-lian2(1.Shaanxi Entry-Exit Inspection and Quarantine Bureau,Xi′an 710068;2.Northwest University,Xi′an 710069);Simultaneous determination of 15 quinolones residues in honey by ultra performance liquid chromatography with electrospray ionization tandem mass spectrometric detection[J];Chinese Journal of Analysis Laboratory;2010-03
5 FEI Jianzhong,HE Rongjun,ZHU Fangming,SUN Peilong(College of Biology and Environmental Engineering,Zhejiang University of Technology, Hangzhou 310014,Zhejiang,China);Progress of molecular imprinted polymer of fluoroquinolones and its application on the food determination[J];Chemical Industry and Engineering Progress;2010-S2
6 Zhao hua,Bian Yongdong,Wang Dexiang,Tang Yong,Huang Chuanguo (Yancheng Quality Supervision and Test Institution of Products,Yanchen224005,China);DETERMINATION OF 20 KINDS OF ANTIBIOTICS RESIDUES IN ANIMAL DERIVED FOOD BY LC-MS/MS[J];Chemical Analysis and Meterage;2011-01
7 YANG Shou-guo1,2 LI Zhao-xin1 WANG Qing-yin1GUO Meng-meng1 TAN Zhi-jun1 XING Li-hong1 YAO Jian-hua1,2(1Yellow Sea Fisheries Research Institute,Chinese Academy of Fishery Sciences,Qingdao 266071)(2College of Fisheries and Life Science,Ocean University of Shanghai,201306);Determination of quinolones drug residues in aquacultural seawater using HPLC method[J];Progress in Fishery Sciences;2010-02
8 DU Liming, WEI Hongqing, ZHANG Junyan, ZHANG Qiaoping (Analytical and Testing Center, Shanxi Normal University, Linfen 041004, China);Separation and Determination of Six Fluoroquinolones by Reversed-Phase High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2003-05
9 DONG Linlin~1, LIU Yanhua~1, WANG Xia~1, ZHONG Feng~1, PENG Li~2, YUE Xiuying~2, GAO Lan~2 (1. China Institute of Veterinary Drug Control, Beijing 100081, China; 2. Sichuan Province Institute of Veterinary Drug Control, Chengdu 610041, China);Simultaneous Determination of Four Fluoroquinolone Residues in Edible Chicken Tissues by Reversed-Phase High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2005-03
10 GUO Genhe, PAN Wei, SU Desen, CHEN Hanzhen(Central Laboratory, Fujian Academy of Agricultural Sciences, Fuzhou 350003, China);Simultaneous Determination of Four Fluoroquinolone Residues in Fish by Ion-Pair High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2005-04
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved