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《Chinese Journal of Analytical Chemistry》 2013-07
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Rapid Screening of Sulfur Fumigated Chinese Star Anises by Surface Desorption Atmospheric Pressure Chemical Ionization Mass Spectrometry

LUO Li-Ping1,WANG Jiang2,ZHANG Wen-Jun3,DAI Xi-Mo1,2,FANG Xiao-Wei2, ZHANG Xi1,2,LIU Ya-Li2,3,CHEN Huan-Wen2 1(School of Life Sciences and Food Engineering,Nanchang University,Nanchang 330047,China) 2(Jiangxi Key Laboratory for Mass Spectrometry and Instrumentation, East China Institute of Technology,Nanchang 330013,China) 3(School of Chemical Engineering,Hebei University of Technology,Tianjin 300130,China)  
Without any sample pretreatment,the mass spectral fingerprints of sulfur fumigated Chinese star anises and untreated samples were rapidly obtained in either a positive or negative ion detection mode with a home-made surface desorption atmospheric pressure chemical ionization(DAPCI) source.The DAPCI-MS raw data were further analyzed by principal component analysis(PCA) and cluster analysis(CA),and several unknown samples were successfully discriminated using the PCA model.The results showed that the DAPCI-MS was able to detect some characteristic chemicals from the Chinese star anises' surface and identify the components by tandem mass spectrometry(MS/MS).The further principal component analysis(PCA) and cluster analysis(CA) of MS fingerprints allow a confident discrimination of sulfur fumigated star anise samples from the non-sulfur fumigated samples.The method developed here is attractive to provide a fast and effective way to screen sulfur fumigated products with sufficient sensitivity and no toxin pollution.This method is expected to be applied to rapid identification of the sulfur fumigated product on the market in future.
【Fund】: “十二五”农村领域国家科技计划基金(No.2012BDA29B01-3);; 国产科学仪器自主创新能力培育与应用示范基金(No.PXM2011_178305_113597);; 江西省科技厅基金(No.2010BNB00900)资助项目
【CateGory Index】: TS264;O657.63
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