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《Journal of Analytical Science》 2002-01
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A Study on the Synthesis of meso-Tetra (5-chloro-4-hydroxyphenyl-3-methoxy) Porphyrin and Its Color Reaction with Fe (Ⅲ)

WANG Yu zhi 1* , LI Qin hong 1, XIONG Jin fang 1, WEN Ning fei 1, DENG Zhi jun 1, ZHOU Wei 2 (1. College of Chemistry and Chemical Engineering, Hunan Univ. Changsha, 410082; 2. Hunan Polytechnical Professional Institute, Changsha, 4100  
A new color reagent, meso tetra (5 chloro 4 hydroxyphenyl 3 methoxy) porphyrin was synthesized. Its spectrophotometric characteristics with Fe (Ⅲ) was studied. In a medium of pH 6.6 buffer and Triton X 100, the orange yellow complex of this reagent with Fe(Ⅲ) was formed. The apparent molar absorptivity of the complex was 6.6×10 5 L·mol -1 ·cm -1 (λ=446 nm). Beer's law was obeyed for Fe (Ⅲ) in the range of 0.01~7.5 μg/25 mL. The reagent has been applied to the determination of Fe (Ⅲ) in the natural water.
【CateGory Index】: O657.3
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