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《Journal of Analytical Science》 2002-02
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The Characterization of L-Cysteine Self-Assembled Monolayers Modified Gold Electrode and Its Differential Pulse Voltametric Response to p-benzenediol

CAI Huo cao, DU Dan, SUN Ya nan, WANG Wei, WANG Sheng fu * (Faculty of Chemistry and Material Science, Hubei University, Wuhan, 430062)  
The electrochemical behaviors of p benzenediol at the L cysteine self assembled monolayers modified gold electrode have been studied. The modified electrode shows an excellent electrocatalytic activity for the oxidation of p benzenediol, making over potential droppen greatly. FTIR and K 3Fe(CN) 6 electrochemical probe were used for the characterization of surface structure of the films. The catalytic current of p benzenediol υs. its concentration has a good linear relation in the range of 2.0×10 -6 ~2.0×10 -4 mol·L -1 , with the correlation coefficient of 0.9986 by differential pulse voltametric response. Detection limit is 4.0×10 -7 mol·L -1 . The modified electrode was used for the determination of p benzenzdiol in imitative water samples with good results.
【Fund】: 湖北省自然科学基金 (No.2 0 0 0 J0 0 7)
【CateGory Index】: O657.1
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