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《Journal of Analytical Science》 2013-03
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Highly Efficient Extraction of Decanoyl Acetaldehyde in Houttuynia cordata thunb under Solvent Immersing

XUE Qing-song *1,YIN Hua-ru 2(1.Shanghai Key Laboratory of Green Chemistry and Chemical Process,Department of Chemistry,East China Normal University,Shanghai 200062;2.Yichuan High School,Shanghai 200061)  
Houttuynia cordata thumb(HCT),the so called antibiotic of traditional Chinese medicine,has been widely employed for clinic therapy.However,the effective extraction of houttuynium(decanoyl acetaldehyde)as a main component of HCT remains an intellectual challenge.In this paper,through the solvent immersing method,the essential oil was extracted,and the influence of reaction conditions on the efficiency of decanoyl acetaldehyde extraction were investigated such as the type of solvents,temperature and time.When ethyl acetate was used as solvent and extraction was processed at room temperature for 456h,the maximum extractability of essential oil was 0.294%,and the content of decanoyl acetaldehyde was up to 40.14%in the essential oil,and only trace of 2-undecanone was found.In the procedure,the mild extraction condition has reduced the decomposition of decanoyl acetaldehyde.The current study provides a promise way to highly effective extraction of decanoyl acetaldehyde from HCT on a large scale.
【CateGory Index】: O658.2;R284.1
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