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《Journal of Analytical Science》 2014-03
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Determination of Methyhestosterone in Aquatic Products by High Performance Liquid Chromatography with Dispersive Solid Phase Extraction

MA Li-sha;ZHU Xin-ping;YIN Yi;DAI Xiao-xin;ZHENG Guang-ming;Pearl River Fishery Research Institute,Chinese Academic of Fishery Science;  
A high performance liquid chromatographic(HPLC)method coupled with dispersive solid phase extraction was established for the determination of methyltestosterone residue in aquatic products.The samples was extracted with ethyl acetate with addition of MgSO4,and then cleaned up by aluminaN.The limit of detection was 8μg/kg,and the method showed a good linearity in the range of 10-10 000ng/mL with a correlation coefficient of 0.9999.And four representative samples(tilapia,grass carp,shrimp and turtle)were used to validate the recovery and precision of the method.The recoveries of methyltestosterone at three spiked levels of 30,50 and 100μg/kg varied from 84.6% to 106%,and the relative standard deviations(RSD)varied from 1.77% to 4.27%.
【Fund】: 中国水产科学研究院院部中央级公益性科研院所基本科研业务费专项(No.2011C008)
【CateGory Index】: O657.72;TS254.7
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【Citations】
Chinese Journal Full-text Database 9 Hits
1 Ma Dan,Gao Lina,Chen Yongping,Li Chunqing;Determination of 17α-methyltestosterone in fish feed by HPLC method[J];Feed Industry;2012-04
2 LIU Jun1,SHEN Jing1,LIU Jian2(1.Agricultural Testing Center & Information Center,Hubei Academy of AgriculturalScience,Wuhan 430064;2.Hubei Province Key Laboratory of Biotechnology ofChinese Traditional Medicine,Hubei University,Wuhan 430062);Determination of Tebuconazole in Straw,Rice,Rice Hull and Soil by Liquid Chromatography-Mass Spectrometry after Dispersive Solid Phase Extraction[J];Journal of Analytical Science;2010-01
3 NIE Jian-rong,ZHU Meng-li,ZHU Ming-li,HE Wen-biao,PAN Yun-shan(Guangzhou agriculture standard and supervisory center,Guangzhou 510315,China);Rapid determination of methyltestosterone in aquaculture with HPLC-MS/MS[J];Guangdong Agricultural Sciences;2008-06
4 CHEN Pei-ji1,LI Liu-dong1,ZOU Qin1,2,LI Zhi-guang1,YANG Jin-lan1,ZHAO Dong-hao1(1.South China Sea Fisheries Research Institute,Chinese Academy of Fishery Sciences,Guangzhou 510300,China;2.College of Food Science and Technology,Guangdong Ocean University,Zhanjiang 524088,China);HPLC Determination of 17α-Methyltestosterone Residue in Aquatic Products[J];Food Science;2010-06
5 ZHU Jing-lin,YANG Hong,XIAO Wei,ZOU Zhi-ying,LI Da-yu,SHAN Hang-yu(Key Laboratory of Freshwater Fisheries and Germplasm Resources Utilization,Ministry of Agriculture,Freshwater Fisheries Research Center,Chinese Academy of Fishery Sciences,Wuxi 214081,China);Determination of Methyltestosterone Residue in Tilapia Muscle by Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry(UPLC-MS/MS)[J];Food Science;2011-22
6 LI Fengge1,2,SU Min1,LI Xiaoyan1,ZHANG Hongxia2,YAO Weiqin1,DOU Hui1,ZHANG Wanquan1(1.Technical Center of Xinjiang Entry-Exit Inspection and Quarantine Bureau,ürümqi 830063,China;2.Food Science Institute,Xinjiang Agricultural University,ürümqi 830063,China);Determination of sulfonamides,quinolones,benzimidazoles and the metabolites of benzimidazoles in chicken livers by dispersive solid-phase extraction and ultra performance liquid chromatography-tandem mass spectrometry[J];Chinese Journal of Chromatography;2011-02
7 SHI Jiawei,LI Jige,WANG Yufei,FAN Jianzhong(Ningbo Key Laboratory of Poison Research and Control,Ningbo Municipal Center for Disease Control and Prevention,Ningbo 315010,China);Analysis of 112 pesticide residues in vegetables using dispersive-solid phase extraction and gas chromatographytriple quadrupole mass spectrometry[J];Chinese Journal of Chromatography;2012-06
8 ZHAO Yonggang,CHEN Xiaohong,YAO Shanshan,LI Xiaoping,JIN Micong(Ningbo Key Laboratory of Poison Research and Control,Ningbo Municipal Center for Disease Control and Prevention,Ningbo 315010,China);Analysis of six phenolic environmental estrogens in bullfrog blood by using dispersive solid-phase extraction and ultrafast liquid chromatographytandem mass spectrometry[J];Chinese Journal of Chromatography;2012-07
9 ZHUO Xiao-Lei1,ZOU Ji-Xing1,CUI Ke1,ZHONG Shan2 and HE Xue-Jun1(1.College of Animal Science,South China Agricultural University,Guangzhou 510642,China;2.Department of Genetics,Basic Medical School of Wuhan University,Wuhan 430071,China);THE INFLUENCE OF EXOGENOUS METHYLTESTOSTERONE ON THE GONAD DEVELOPMENTAL PROCESS OF FEMALE AND INTERSEXUAL MONOPTERUS ALBUS[J];Acta Hydrobiologica Sinica;2008-06
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 SUN Hui et al(College of Resources and Environment,Jilin Agricultural University,Changchun,Jilin 130118);Studies on Residue Analysis Method of Tebuconazole in Soybean by Gas Chromatography[J];Journal of Anhui Agricultural Sciences;2011-15
2 TANG Jie1,YUE Yong-de2,TANG Feng2,HUA Ri-mao1(1.School of Resources and Environment,Anhui Agricultral University,Hefei 230036; 2.International Center for Bamboo & Rattan,Beijing 100080);Method for residue analysis of tebuconazole in wheat with GC[J];Journal of Anhui Agricultural University;2011-03
3 HONG Er-li1,2,ZHENG Guang-ming2*,MENG Di3,WU Shi-hui2,DAI Xiao-xin2,MA Bing3,MA Li-sha,SONG Yi3(1.Faculty of Fisheries and Life Science,Shanghai Ocean University,Shanghai 200090; 2.Pearl River Fishery Research Institute,Chinese Academic of Fishery Science,Guangzhou 510380;, 3.Chinese Academic of Fishery Science,Beijing 100141);Pharmacokinetics and elimination of methyl testosterone in tilapia[J];Journal of Anhui Agricultural University;2011-06
4 Ma Dan,Gao Lina,Chen Yongping,Li Chunqing;Determination of 17α-methyltestosterone in fish feed by HPLC method[J];Feed Industry;2012-04
5 WU Fang-hua(Fuzhou Product Quality Inspection,Fuzhou 350002,China);Study of New Technology on Solid Phase Extraction[J];Analysis and Testing Technology and Instruments;2012-02
6 LUO Hui-Tai,HUANG Xiao-Lan,WU Hui-Qin,ZHU Zhi-Xin,HUANG Fang,LIN Xiao-Shan(Guangdong Provincial Public Laboratory of Analysis and Testing Technology, China National Analytical Center(Guangzhou),Guangzhou 510070);Simultaneous Determination of 33 Medicine Residues in Aquatic Products by Rapid Resolution Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2012-02
7 ZHAO Jing,GAO Jin,WU Yu-kuan,TANG Che,YANG Yan, YU Jing,YAN Gui-fang(Hubei Inspection Center for Agri-food Quality & Safety,Wuhan 430070);Dtermination of 18 Pesticides in Vegetables Using High Performance Liquid Chromatography-Electrospray Ionization Tandem Mass Spectrometry[J];Journal of Analytical Science;2011-06
8 HUANG Zhi-bo,WU Chun-mei,LI Jing-zhao,CHEN Jian-hang,CHENG Xue-mei(Dongguan Agricultural Products Institute of Quality Safety Supervision and Inspection,Dongguan 523000,China);SPE UPLC-MS/MS determination of residual of 7 kinds of microbicides in vegetables[J];Guangdong Agricultural Sciences;2011-24
9 Xue Li1,He Huimin1,Li Xiaozhi1,Li Ouyan2,Cheng Miaojin2,Wen Qin2(1.Guangdong Research Institute of Petrochemical Industry,Guangzhou 510665;2.Shenzhen Noposion Pesticides Stock Co.,Shenzhen 518102,China);Analysis of Azoxystrobin and Tebuconazole in SC by UPLC[J];Guangdong Chemical Industry;2012-08
10 ZHANG Yong,ZHANG Bei-bei,ZHAO Yong-gang(State Environmental Protection Key Laboratory of Monitoring and Analysis for Organic Pollutants in Surface Water,Environment Monitoring Center of Jiangsu Province,Jiangsu Nanjing 210036,China);Determination of Tebuconazole in Water Using Ultra-HPLC-Electrospray Tandem Mass Spectrometry[J];Guangzhou Chemical Industry;2012-17
China Proceedings of conference Full-text Database 3 Hits
1 DENG Jian-chao,YANG Xian-qing,LI Lai-hao,WU Yan-yan,CEN Jian-wei,CHEN Sheng-jun,Qi Bo (South China Sea Fisheries Research Institute,Chinese Academy of Fishery Sciences;Key Laboratory of Aquatic Products Processing.Ministry of Agriculture,Guangzhou 510300,China);Determination of 17a-Methyltestosterone Residue in Aquatic Water and Sediment by High Performance Liquid Chromatography[A];[C];2012
2 ZHANG,Kan-kan SONG,Bao-An~* YANG,Song (State Key Laboratory Breeding Base of Green Pesticide and Agricultural Bioengineering,Key Laboratory of Green Pesticide and Agriculture Bioengineering,Ministry of Education,Center for Research and Development of Fine Chemicals,Guizhou University,Guiyang 550025,China);Research Overview on Analysis of Chiral Pesticides[A];[C];2010
3 Nan Feng;Beijing Municipal Center for Food Safety Monitoring and Risk Assessment;;Research for 85 Toxic and Harmful Substances in Food Screening Technology[A];[C];2014
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 L Dao-Yuan 1, SONG Ping [DK3]1** , CHEN Yun-Gui 1, PENG Mao-Yu 1,GUI Jian-Fang 2 1. School of Life Sciences Wuhan University, Wuhan 430072, China 2. State Key Laboratory of Freshwater Ecology and Biotechnology, Institute of Hydrobiology, Chinese Academy of Sciences, Wuhan 430072, China;Expression of gene vasa during gonadal natural sex reversal of ricefield eel Monopterus albus[J];Acta Zoologica Sinica;2005-03
2 YANG Wen-yun~(1), GU Zhong-qi~(2), WANG Chun-hua~(3), DONG Wu-zi~(2) (1. Gansu National Nature Sanctuary Management Bureau ,Wenxian,Gansu,746400,China; 2.The Animal Sci-tech College of the Northwest Sci-tech University of Agriculture and Forestry,Yangling, Shaanxi,712100,China; 3.Shandong Longkou Dongjiang Veterinary Station,Longkou,Shandong,265718,China);Observation of Gonad Histology in the Course of the Sex Reverses for the Eels(Homopterous albums)[J];Progress In Veterinary Medicine;2004-06
3 HUANG Xiao-dong, LIN Zi-an, XIE Zeng-hong (College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, Fujian 350002, China; Chemistry and Chemical Engineering Department of Minjiang University, Fuzhou, Fuiian 350002, China);Determination of Metbyltestosterone with Capillary Electrophoresis[J];Journal of Minjiang University;2006-02
4 Pang Guofang~, Cao Yanzhong, Zhang Jinjie, Jia Guangqun, Fan Chunlin, Li Xuemin, Liu Yongming, Shi Yuqiu (Qinhuangdao Entry-Exit Inspection and Quarantine Bureau, Qinhuangdao 066002);Simultaneous Determination of 16 Sulfonamides in Poultry Meat by High-Performance Liquid Chromatography- Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2005-09
5 Zhao Si-Jun, Li Cun, Jiang Hai-Yang, Li Bing-Yu, Shen Jian-Zhong(College of Veterinary Medicine, China Agricultural University, Beijing 100094);Simultaneous Determination of 7 Quionlones Residues in Animal Muscle Tissues by High Performance Liquid Chromatography[J];Chinese Journal of Analytical Chemistry;2007-06
6 YANG Hong~(*1), GUO Hua~(1), ZHAO Wei-jia~(1), WU Jiu-qing~(2), ZHOU Guang-hong~(2) (1. College of Science, Nanjing Agricultural University; 2. College of Food Science and Technology, Nanjing Agricultural University, Nanjing 210095);Study on Analysis of Pesticide Multiresidues in Milk[J];Journal of Analytical Science;2005-02
7 ZENG Dan-yun,JI Xing-hu,HE Zhi-ke~*(College of Chemistry & Molecular Sciences,Wuhan University,Wuhan 430072);Chemiluminescence Determination of Methyltestosterone with Methyltestosterone-KMnO_4-Ru(bipy)_3~(2+)-Ce(Ⅳ) System[J];Journal of Analytical Science;2005-05
8 LIN Hai-dan, XIE Shou-xin and WU Ying-xuan (Technical Center for Inspection & Quarantine on Food of Guangzhou CIQ, Guangzhou 510623);Determination of benzimidazoles veterinary drug residues in milk powder by SPE-HPLC[J];Analytical Laboratory;2005-01
9 NIE Jian-rong,ZHU Meng-li,ZHU Ming-li,HE Wen-biao,PAN Yun-shan(Guangzhou agriculture standard and supervisory center,Guangzhou 510315,China);Rapid determination of methyltestosterone in aquaculture with HPLC-MS/MS[J];Guangdong Agricultural Sciences;2008-06
10 ZHOU Qiu-bai, WU Hua-dong, WU Hong-xiang, PANG Hui-zhong, LE Shi-Iiang (1. Department of Animal Science and Technology, Jiangxi Agricultural University, Nanchang 330045, China; 2. Analyzing and Detecting Center of Jiangxi Agricultural University, Nanchang 330045, China ; 3. Shangrao County Xiapei Animal Breed Farm, Shangrao 334100, China);The Effect of Spawn and Not Spawn on Sex Reversal in Ricefield Eel[J];Journal of Economic Animal;2004-02
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